作者: Gopal Avashthi , Shrikant S. Maktedar , Man Singh
DOI: 10.1063/5.0001724
关键词: Thermal stability 、 Thermogravimetric analysis 、 Fourier transform infrared spectroscopy 、 Materials science 、 Nuclear chemistry 、 Infrared spectroscopy 、 Graphene 、 Absorption spectroscopy 、 Oxide 、 X-ray photoelectron spectroscopy
摘要: Sonochemical method has been used for graphene oxide functionalization (f-GrO). The acoustic cavitation acts as a small reactor to induce in-situ temperature (T) GrO with 5-Amino-1,3,4-thiadiazole-2-thiol (ATDT) [f-(ATDT)GrO] nitrogen functionalized (N-f-GrO). thermal stability (TS) of N-f-GrO was confirmed using thermogravimetric analysis (TGA) total % wt. loss 51.7 at 231.8 °C. establishment new electronic entities in X-ray photoelectron spectroscopy (XPS), Soft absorption (SXAS), diffraction (XRD). characteristics functional groups were Fourier-transform infrared (FTIR) and 13C solid-state NMR (SSNMR). Insight structural cell viabilities 10-80 µg/ml on MCF-7 Vero lines observed average values 98.02 88.65 respectively Sulforhodamine B (SRB) assay.