Application of LC–MS and LC–NMR Techniques for Secondary Metabolite Identification
作者： Tristan Richard , Hamza Temsamani , Emma Cantos-Villar , Jean-Pierre Monti
DOI: 10.1016/B978-0-12-397922-3.00002-2
关键词: Liquid chromatography–mass spectrometry 、 Chromatography 、 Mass spectrometry 、 Secondary metabolite 、 Biology
摘要: Abstract An overview of advancements and applications liquid chromatography coupled to nuclear magnetic resonance (LC–NMR) is given discussed for secondary metabolites in the plant kingdom: terpenoids, alkaloids phenolic compounds. The different LC–NMR operating modes are presented order structure compound elucidation. On-flow stop-flow described, together with technical improvements such as LC–SPE–NMR capLC–NMR. Synergetic combination hyphenated techniques mass spectrometry NMR illustrated an example.
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