Determination of Total Mercury in Solid Samples by Anodic Stripping Voltammetry
作者： Huyen Thu Luu , Thao Thi Ta , Loi Duc Vu , Thuong Thi Kim Nguyen , Giang Thi Huong Le
DOI: 10.1155/2021/8888879
关键词: Electrode 、 Detection limit 、 Mass spectrometry 、 Mercury (element) 、 Deposition (phase transition) 、 Chemistry 、 Anodic stripping voltammetry 、 Cold vapour atomic fluorescence spectroscopy 、 Peak current 、 Analytical chemistry
摘要: The anodic stripping voltammetry (ASV) was investigated to determine total mercury in solid samples using a gold electrode. deposited on the electrode preconcentration step. oxidation peak of irreversible. optimal conditions procedure were found be as follows: 0.05 mol L−1 HCl solution, deposition potential −0.5 V vs. Ag/AgCl/KCls, time 40 s, and sweep rate 0.04 V s−1. Under conditions, current showed linear dependence Hg2+ concentration range from 0.01 0.1 mg l−1. detection limit quantification 4.28 µg L−1 12.98 µg L−1, respectively. mean recovery relative standard deviation 91.2% 2.4% (n = 9). successfully applied for determining collected Hanoi light bulb warehouse—The Rang Dong Light Source Vacuum Flask JSC. results compared with cold vapor atomic absorption spectrometry (CV-AAS).
hindawi.com参考文章(44)
Edyta KOPYSC, Krystyna PYRZYNSKA, Slawomir GARBOS, Ewa BULSKA, Determination of mercury by cold-vapor atomic absorption spectrometry with preconcentration on a gold-trap Analytical Sciences. ,vol. 16, pp. 1309- 1312 ,(2000) , 10.2116/ANALSCI.16.1309
Juan Sánchez, Elianna Castillo, Piedad Corredor, Jesús Ágreda, None, Determination of Mercury by Anodic Stripping Voltammetry in Aqua Regia Extracts Portugaliae Electrochimica Acta. ,vol. 29, pp. 197- 210 ,(2011) , 10.4152/PEA.201103197
Elisabeth G. Pacyna, Jozef M. Pacyna, Frits Steenhuisen, Simon Wilson, Global anthropogenic mercury emission inventory for 2000 Atmospheric Environment. ,vol. 40, pp. 4048- 4063 ,(2006) , 10.1016/J.ATMOSENV.2006.03.041
Marie Vahter, Agneta Åkesson, Birger Lind, Ulla Björs, Andrejs Schütz, Marika Berglund, Longitudinal study of methylmercury and inorganic mercury in blood and urine of pregnant and lactating women, as well as in umbilical cord blood. Environmental Research. ,vol. 84, pp. 186- 194 ,(2000) , 10.1006/ENRS.2000.4098
Fenglian Xu, Svetlana Farkas, Simone Kortbeek, Fang-Xiong Zhang, Lina Chen, Gerald W Zamponi, Naweed I Syed, Mercury-induced toxicity of rat cortical neurons is mediated through N-methyl-D-Aspartate receptors Molecular Brain. ,vol. 5, pp. 30- 30 ,(2012) , 10.1186/1756-6606-5-30
Adil Mandil, Laila Idrissi, Aziz Amine, Stripping voltammetric determination of mercury(II) and lead(II) using screen-printed electrodes modified with gold films, and metal ion preconcentration with thiol-modified magnetic particles Mikrochimica Acta. ,vol. 170, pp. 299- 305 ,(2010) , 10.1007/S00604-010-0329-X
Issa Touridomon Somé, Abdoul Karim Sakira, Dominique Mertens, Sebastien N. Ronkart, Jean-Michel Kauffmann, Determination of groundwater mercury (II) content using a disposable gold modified screen printed carbon electrode Talanta. ,vol. 152, pp. 335- 340 ,(2016) , 10.1016/J.TALANTA.2016.02.033
Tshia Malehase, Adegbenro P. Daso, Jonathan O. Okonkwo, Determination of mercury and its fractionation products in samples from legacy use of mercury amalgam in gold processing in Randfontein, South Africa Emerging Contaminants. ,vol. 2, pp. 157- 165 ,(2016) , 10.1016/J.EMCON.2016.07.003
Shirley LE ROUX, Priscilla BAKER, Andrew CROUCH, Determination of mercury in selected polluted sediments using HPLC-ICP-MS in Westbank area, Western Cape, South Africa South African journal of chemistry. ,vol. 69, pp. 124- 131 ,(2016) , 10.17159/0379-4350/2016/V69A15
Armin Fashi, Mohammad Reza Yaftian, Abbasali Zamani, Electromembrane extraction-preconcentration followed by microvolume UV–Vis spectrophotometric determination of mercury in water and fish samples Food Chemistry. ,vol. 221, pp. 714- 720 ,(2017) , 10.1016/J.FOODCHEM.2016.11.115