High-performance liquid chromatographic method with quantitative comparisons of whole chromatograms of raw and steamed Panax notoginseng.

作者: Aik-Jiang Lau , Bee-Hong Seo , Soo-On Woo , Hwee-Ling Koh

DOI: 10.1016/J.CHROMA.2004.09.069

关键词: Raw materialPanax notoginsengQuantitative analysis (chemistry)Medicinal herbsSteam distillationHigh-performance liquid chromatographyChromatographyChemistryChemical fingerprintingSteaming

摘要: A high-performance liquid chromatographic (HPLC) method coupled with pattern matching was developed to differentiate whole chromatograms of raw and steamed Panax notoginseng objectively quantitatively. The major peaks differentiating samples were also identified for the first time in this herb. P. roots its products successfully differentiated. quantitative differences between correlated duration steaming. Chromatographic allows rapid, simple, automated, comparisons complex chromatograms. It is a useful tool ensuring safety quality herbal products.

参考文章(16)
Norman R. Farnsworth, Harry Hong Sang Fong, Gail B. Mahady, Botanical dietary supplements: quality, safety and efficacy. Botanical dietary supplements: quality, safety and efficacy.. ,(2001)
Rongwei Teng, Haizhou Li, Jiangtao Chen, Dezu Wang, Yineng He, Chongren Yang, Complete assignment of 1H and 13C NMR data for nine protopanaxatriol glycosides Magnetic Resonance in Chemistry. ,vol. 40, pp. 483- 488 ,(2002) , 10.1002/MRC.1033
J Quesada Granados, Juan-Julián Merelo Guervós, MJ Oliveras López, J González Peñalver, M Olalla Herrera, R Blanca Herrera, MC López Martinez, None, Application of artificial aging techniques to samples of rum and comparison with traditionally aged rums by analysis with artificial neural nets. Journal of Agricultural and Food Chemistry. ,vol. 50, pp. 1470- 1477 ,(2002) , 10.1021/JF010889I
Kevin J. Johnson, Bob W. Wright, Kristin H. Jarman, Robert E. Synovec, High-speed peak matching algorithm for retention time alignment of gas chromatographic data for chemometric analysis Journal of Chromatography A. ,vol. 996, pp. 141- 155 ,(2003) , 10.1016/S0021-9673(03)00616-2
Fan Gong, Yi-Zeng Liang, Pei-Shan Xie, Foo-Tim Chau, Information theory applied to chromatographic fingerprint of herbal medicine for quality control Journal of Chromatography A. ,vol. 1002, pp. 25- 40 ,(2003) , 10.1016/S0021-9673(03)00648-4
Ralf J. O. Torgrip, Magnus Åberg, Bo Karlberg, Sven P. Jacobsson, Peak alignment using reduced set mapping Journal of Chemometrics. ,vol. 17, pp. 573- 582 ,(2003) , 10.1002/CEM.824
William J. Welsh, Wangkan Lin, Samuel H. Tersigni, Elizabeth Collantes, Radu Duta, Michael S. Carey, Walter L. Zielinski, James Brower, John A. Spencer, Thomas P. Layloff, Pharmaceutical Fingerprinting: Evaluation of Neural Networks and Chemometric Techniques for Distinguishing among Same-Product Manufacturers Analytical Chemistry. ,vol. 68, pp. 3473- 3482 ,(1996) , 10.1021/AC951164E
Fan Gong, Yi-Zeng Liang, Ying-Sing Fung, Foo-Tim Chau, Correction of retention time shifts for chromatographic fingerprints of herbal medicines Journal of Chromatography A. ,vol. 1029, pp. 173- 183 ,(2004) , 10.1016/J.CHROMA.2003.12.049
Christophe BY Cordella, Julio SLT Militão, Marie-Claude Clément, Daniel Cabrol-Bass, None, Honey characterization and adulteration detection by pattern recognition applied on HPAEC-PAD profiles. 1. Honey floral species characterization. Journal of Agricultural and Food Chemistry. ,vol. 51, pp. 3234- 3242 ,(2003) , 10.1021/JF021100M