Preparation of (perfluoroalkyl)alkane thiols via Zemplén deacylation of fluorous (perfluoroalkyl)alkyl thioacetates

作者: Bálint Menczinger , Anikó Nemes , Csongor Szíjjártó , József Rábai

DOI: 10.1016/J.JFLUCHEM.2018.02.014

关键词: Medicinal chemistryChemistryAlkylPotassium thioacetateAlkane

摘要: … -(p-C 8 F 17 CH 2 CH 2 SC 6 F 4 ) 4 porH 2 ] showed quantum interferences in molecule … Air/water bubble stabilization was effected with C 6 F 13 CH 2 CH 2 (OCH 2 CH 2 ) 4 SH type …

参考文章(56)
J. L. Wardell, Preparation of thiols The Thiol Group: Volume 1(1974). pp. 163- 269 ,(2010) , 10.1002/9780470771310.CH4
József Rábai, Fun and Games with Fluorous Chemistry Wiley‐VCH Verlag GmbH & Co. KGaA. pp. 574- 585 ,(2005) , 10.1002/3527603905.CH14
Cheng-Pan Zhang, Zhenxing Xi, Kory M. Mueller, Bradley J. Holliday, Hassan S. Bazzi, John A. Gladysz, Phase and redox shifted four iron/four sulfur clusters: fluorous analogs of metalloenzyme cofactors Dalton Transactions. ,vol. 44, pp. 19615- 19624 ,(2015) , 10.1039/C5DT01959A
Mathias Brust, Merryl Walker, Donald Bethell, David J. Schiffrin, Robin Whyman, Synthesis of thiol-derivatised gold nanoparticles in a two-phase liquid-liquid system Journal of The Chemical Society, Chemical Communications. pp. 801- 802 ,(1994) , 10.1039/C39940000801
Joseph H. Simons, The Seven Ages of Fluorine Chemistry Journal of Fluorine Chemistry. ,vol. 32, pp. 7- 24 ,(1986) , 10.1016/S0022-1139(00)80503-5
Oussama Zenasni, Andrew C. Jamison, T. Randall Lee, The impact of fluorination on the structure and properties of self-assembled monolayer films Soft Matter. ,vol. 9, pp. 6356- 6370 ,(2013) , 10.1039/C3SM00054K
Tomáš Bříza, Vladimír Král, Pavel Martásek, Robert Kaplánek, Electrophilic polyfluoroalkylating agents based on sulfonate esters Journal of Fluorine Chemistry. ,vol. 129, pp. 235- 247 ,(2008) , 10.1016/J.JFLUCHEM.2007.11.009
Kym Ford, Bronwyn J. Battersby, Barry J. Wood, Ian R. Gentle, The production and verification of pristine semi-fluorinated thiol monolayers on gold. Journal of Colloid and Interface Science. ,vol. 370, pp. 162- 169 ,(2012) , 10.1016/J.JCIS.2011.10.081
Natacha Mureau, Frédéric Guittard, Serge Géribaldi, Convenient synthesis of thiols and disulfides in the polyfluorinated series incorporating a butylic spacer Tetrahedron Letters. ,vol. 41, pp. 2885- 2889 ,(2000) , 10.1016/S0040-4039(00)00303-8