Process for the distillation of crude ester in the DMT/PTA process

作者: Ulrich Neutzler , Anton Schoengen , Reinhard Dr. Sigg , Udo Lenz

DOI:

关键词: ChromatographyContinuous distillationFractionating columnDistillationStructured packingOrganic chemistryYield (chemistry)MethanolDimethyl terephthalateChemistryOxidizing agent

摘要: A process for preparing crude dimethyl terephthalate, comprises oxidizing a mixture comprising para-xylene and methyl para-toluate, esterifying the oxidized with methanol, separating resulting ester into fractions. By distillation column containing structured packing using lower bottom temperature, product yield is increased, made more economical.

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