作者: Ulrich Neutzler , Anton Schoengen , Reinhard Dr. Sigg , Udo Lenz
DOI:
关键词: Chromatography 、 Continuous distillation 、 Fractionating column 、 Distillation 、 Structured packing 、 Organic chemistry 、 Yield (chemistry) 、 Methanol 、 Dimethyl terephthalate 、 Chemistry 、 Oxidizing agent
摘要: A process for preparing crude dimethyl terephthalate, comprises oxidizing a mixture comprising para-xylene and methyl para-toluate, esterifying the oxidized with methanol, separating resulting ester into fractions. By distillation column containing structured packing using lower bottom temperature, product yield is increased, made more economical.