HEADSPACE TECHNIQUES IN MOUTH ODOR ANALYSIS

作者: D.A.M. Mackay , M.M. Hussein

DOI: 10.1016/B978-0-12-169050-2.50019-3

关键词: Mouth breathOral cavityFlow resistanceElutionOdorChromatographyChemistry

摘要: Breath was analyzed for its sulfur-containing organic volatiles before and after ingestion of a number foods, using various headspace gas chromatographic techniques the flame photometric detector (FPD). These included direct injection, head space concentration via use short pre-columns (both porous polymer coated support types), also very long open columns low flow resistance. Elution absorbed from these into analytical column studied. Use standard pre-column, as an intermediate step to collect stripped pre-columns, permitted collection levels large volumes unimpeded “lung breath”. The pre-column used oral cavity, 40 cc “mouth

参考文章(30)
J. W. Rhoades, Coffee Volatiles, Analysis of the Volatile Constituents of Coffee Journal of Agricultural and Food Chemistry. ,vol. 8, pp. 136- 141 ,(1960) , 10.1021/JF60108A019
M.H. Brodnitz, C.L. Pollock, Gas chromatographic analysis of distilled onion oil Food Technology. ,vol. 24, pp. 78- 80 ,(1970)
J. Tonzetich, P.W. Johnson, Chemical analysis of thiol, disulphide and total sulphur content of human saliva Archives of Oral Biology. ,vol. 22, pp. 125- 131 ,(1977) , 10.1016/0003-9969(77)90089-9
B. Krotoszynski, G. Gabriel, H. O'Neill, M. P. A. Claudlo, Characterization of Human Expired Air: A Promising Investigative and Diagnostic Technique Journal of Chromatographic Science. ,vol. 15, pp. 239- 244 ,(1977) , 10.1093/CHROMSCI/15.7.239
John W. Russell, Analysis of air pollutants using sampling tubes and gas chromatography Environmental Science & Technology. ,vol. 9, pp. 1175- 1178 ,(1975) , 10.1021/ES60111A011
J. Tonzetich, Direct gas chromatographic analysis of sulphur compounds in mouth air in man Archives of Oral Biology. ,vol. 16, pp. 587- 597 ,(1971) , 10.1016/0003-9969(71)90062-8
P. S. Farrington, R. L. Pecsok, R. L. Meeker, T. J. Olson, Detection of Trace Constituents by Gas Chromatography. Analysis of Polluted Atmosphere Analytical Chemistry. ,vol. 31, pp. 1512- 1516 ,(1959) , 10.1021/AC60153A029
James P. Conkle, Bennie J. Camp, Billy E. Welch, Trace composition of human respiratory gas. Archives of Environmental Health. ,vol. 30, pp. 290- 295 ,(1975) , 10.1080/00039896.1975.10666702
A. J. Macleod, Glesni Macleod, Volatiles of cooked cabbage Journal of the Science of Food and Agriculture. ,vol. 19, pp. 273- 277 ,(1968) , 10.1002/JSFA.2740190509