Extraction methodology and chromatography for the determination of residual pesticides in water

作者: Štefan Hatrík , Jozef Tekel'

DOI: 10.1016/0021-9673(95)00725-3

关键词: Residue (complex analysis)Extraction (chemistry)ChemistryDetection limitPesticide residuePesticideGas chromatographyChromatographyEnvironmental chemistrySupercritical fluid extractionEnvironmental analysis

摘要: The contemporary state of the determination pesticide residues and some their transformation products is reviewed. review covers chromatographic herbicides, insecticides important fungicide toxic (substituted anilines, chlorophenols, ethylenethiourea) in various types water samples. Advantages drawbacks gas liquid chromatography this type analysis are discussed. emphasis placed on multi-residue analytical methods with required limit quantification (LOQ < 0.1 μg l−1) recovery. Various aspects isolation, preconcentration clean-up residue extracts from samples discussed (liquid-liquid extraction, liquid-solid extraction supercritical fluid extraction). characteristics a modern method for summarized trends development GC LC

参考文章(102)
Jozef Kováč, Jozef Tekel, Magda Kurucová, Determination of herbicide residues in agricultural crops, foods, soil and water by chronometric method. European Food Research and Technology. ,vol. 184, pp. 96- 100 ,(1987) , 10.1007/BF01042081
Antonio Di Corcia, Stefano Marchese, Roberto Samperi, Giancarlo Cecchini, Luciano Cirilli, Determination of Phenol Pollutants in Water at Trace Levels: Extraction by a Reversible Graphitized Carbon Black Cartridge Journal of AOAC International. ,vol. 77, pp. 446- 453 ,(1994) , 10.1093/JAOAC/77.2.446
J. F. Copplestone, The development of the WHO Recommended Classification of Pesticides by Hazard. Bulletin of The World Health Organization. ,vol. 66, pp. 545- 551 ,(1988)
Verne A. Simon, Anne Taylor, High-sensitivity high-performance liquid chromatographic analysis of diquat and paraquat with confirmation Journal of Chromatography A. ,vol. 479, pp. 153- 158 ,(1989) , 10.1016/S0021-9673(01)83326-4
C.E. Goewie, P. Kwakman, R.W. Frei, U.A.Th. Brinkman, W.Maasfeld T. Seshadri, A. Kettrup, Pre-column technology in high-performance liquid chromatography for the determination of phenylurea herbicides in water in the presence of their anilines Journal of Chromatography A. ,vol. 284, pp. 73- 86 ,(1984) , 10.1016/S0021-9673(01)87803-1
Peter. Klaffenbach, Patrick T. Holland, Analysis of sulfonylurea herbicides by gas-liquid chromatography. 2. Determination of chlorsulfuron and metsulfuron-methyl in soil and water samples Journal of Agricultural and Food Chemistry. ,vol. 41, pp. 396- 401 ,(1993) , 10.1021/JF00027A010
S.A. Schuette, R.G. Smith, L.R. Holden, J.A. Graham, Solid-phase extraction of herbicides from well water for determination by gas chromatography-mass spectrometry Analytica Chimica Acta. ,vol. 236, pp. 141- 144 ,(1990) , 10.1016/S0003-2670(00)83307-3
Thomas R. Steinheimer, HPLC determination of atrazine and principal degradates in agricultural soils and associated surface and ground water Journal of Agricultural and Food Chemistry. ,vol. 41, pp. 588- 595 ,(1993) , 10.1021/JF00028A016
S. Chiron, E. Martinez, D. Barceló, On-line and off-line sample preparation of acidic herbicides and bentazone transformation products in estuarine waters Journal of Chromatography A. ,vol. 665, pp. 283- 293 ,(1994) , 10.1016/0021-9673(94)85058-5