Characteristic structural features of cyclopentadienyl derivatives of post-transition metals
作者： T.V. Baukova , Yu.L. Slovokhotov , Yu.T. Struchkov
DOI: 10.1016/S0022-328X(00)88380-1
关键词: Cyclopentadienyl complex 、 Chemistry 、 Benzene 、 Diffraction 、 Cationic polymerization 、 Transition metal 、 Crystallography 、 Triclinic crystal system 、 Group (periodic table)
摘要: Abstract The trinuclear cationic complex [Ph4C5(AuPPh3)3+[BF4]- (I) obtained by interaction of C5HPh4AuPPh3 or Ph4C5(AuPPh3)2 with [AuPPh3+[BF4]- in THF was studied X-ray diffraction. In the presence benzene, triclinic crystals solvate [Ph4C5(AuPPh3)3]+[BF4]-· 2 C6H6 are formed, a = 12.845(6), b 16.042(8), c 22.642(11) A, α 86.62(4), β 77.51(4), γ 76.05(4)°, space group P 1 , Z 2, 9494 reflections I > 2σ (λ(Mo-Kα), θ/2θ scan, 2θ
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