Synthesis and characterization of ZnO incorporated magnetically recoverable KIT-6 as a novel and efficient catalyst in the preparation of symmetrical N, N′-alkylidene bisamides
作者： Hamid Reza Saadati-Moshtaghin , Farrokhzad Mohammadi Zonoz , Mostafa M Amini , None
DOI: 10.1016/J.JSSC.2018.01.014
关键词: Transmission electron microscopy 、 Mesoporous material 、 Condensation reaction 、 Nanocomposite 、 Infrared 、 Mesoporous silica 、 Chemical engineering 、 Diffraction 、 Catalysis 、 Materials science
摘要: Abstract A novel magnetically recoverable nanocomposite consisting of the NiFe2O4 core and KIT-6 mesoporous silica shell incorporated with ZnO nanoparticles was constructed. This characterized by Fourier transform infrared (FT-IR), powder X-ray diffraction (XRD), Brunauer Emmett Teller (BET), field emission scanning electron microscopy (FESEM), transmission (TEM) vibrating sample magnetometry (VSM). new demonstrated a catalytic performance in synthesis symmetrical N,N′-alkylidene bisamides at condensation reaction under solvent-free conditions. The nanocatalyst could simply be recovered from environment using an exterior magnet reused five times without remarkable losing property.
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sci-hub.se 参考文章(37)
Behrooz Maleki, Farrokhzad Mohammadi Zonoz, Hossien Ali Akhlaghi, An Efficient Synthesis of Symmetrical N,N′-Alkylidene bis-Amides Catalyzed by a Heteropolyacid Organic Preparations and Procedures International. ,vol. 47, pp. 361- 367 ,(2015) , 10.1080/00304948.2015.1066646
Mohammad Reza Mohammad Shafiee, None, Silica-supported barium chloride (SiO2–BaCl2) — Efficient and heterogeneous catalyst for the environmentally friendly preparation of N,N′-alkylidene bisamides under solvent-free conditions Canadian Journal of Chemistry. ,vol. 89, pp. 555- 561 ,(2011) , 10.1139/V11-007
Xiao Xia Shen, Ying Lin Shen, Yi Feng Han, Qiang Liu, None, Synthesis of Symmetrical N,N′-Alkylidene Bisamides Using Zinc Chloride as a Lewis Acid Catalyst Advanced Materials Research. ,vol. 441, pp. 421- 425 ,(2012) , 10.4028/WWW.SCIENTIFIC.NET/AMR.441.421
M. Masteri-Farahani, F. Farzaneh, M. Ghandi, Synthesis and characterization of a new epoxidation catalyst by grafting cis-MoO2(salpr) complex to functionalized MCM-41 Journal of Molecular Catalysis A-chemical. ,vol. 243, pp. 170- 175 ,(2006) , 10.1016/J.MOLCATA.2005.08.013
Piaoping Yang, Zewei Quan, Chunxia Li, Hongzhou Lian, Shanshan Huang, Jun Lin, None, Fabrication, characterization of spherical CaWO4:Ln @MCM-41(Ln = Eu3+, Dy3+, Sm3+, Er3+) composites and their applications as drug release systems Microporous and Mesoporous Materials. ,vol. 116, pp. 524- 531 ,(2008) , 10.1016/J.MICROMESO.2008.05.016
M. Mohammadikish, M. Masteri-Farahani, S. Mahdavi, Immobilized molybdenum–thiosemicarbazide Schiff base complex on the surface of magnetite nanoparticles as a new nanocatalyst for the epoxidation of olefins Journal of Magnetism and Magnetic Materials. ,vol. 354, pp. 317- 323 ,(2014) , 10.1016/J.JMMM.2013.11.013
Alireza Nezamzadeh-Ejhieh, Fatemeh Khodabakhshi-Chermahini, Incorporated ZnO onto nano clinoptilolite particles as the active centers in the photodegradation of phenylhydrazine Journal of Industrial and Engineering Chemistry. ,vol. 20, pp. 695- 704 ,(2014) , 10.1016/J.JIEC.2013.05.035
Amir Khojastehnezhad, Mohammad Rahimizadeh, Hossein Eshghi, Farid Moeinpour, Mehdi Bakavoli, Ferric hydrogen sulfate supported on silica‐coated nickel ferrite nanoparticles as new and green magnetically separable catalyst for 1,8‐dioxodecahydroacridine synthesis Chinese Journal of Catalysis. ,vol. 35, pp. 376- 382 ,(2014) , 10.1016/S1872-2067(14)60001-2
Anand Ramanathan, Rajamanickam Maheswari, Dewey H. Barich, Bala Subramaniam, Niobium incorporated mesoporous silicate, Nb-KIT-6: Synthesis and characterization Microporous and Mesoporous Materials. ,vol. 190, pp. 240- 247 ,(2014) , 10.1016/J.MICROMESO.2014.02.019
Mohammad Anary-Abbasinejad, Mohammad H. Mosslemin, Alireza Hassanabadi, Safiyeh Tajik Safa, p-Toluene Sulfonic Acid–Catalyzed, Solvent-Free Synthesis of Symmetrical Bisamides by Reaction Between Aldehydes and Amides Synthetic Communications. ,vol. 40, pp. 2209- 2214 ,(2010) , 10.1080/00397910903219617