Synthesis growth and characterization of l-valine nickel (II) chloride
作者： M. K. Sangeetha , M. Mariappan , G. Madhurambal , S. C. Mojumdar
DOI: 10.1007/S10973-012-2355-X
关键词: Crystal 、 Infrared 、 Nickel 、 Nickel(II) chloride 、 Crystallography 、 Analytical chemistry 、 Thermal analysis 、 Chloride 、 Thermogravimetric analysis 、 Evaporation (deposition) 、 Materials science
摘要: A new semi organic nonlinear optical crystal, l-valine nickel chloride has been synthesized and good quality single crystals were grown by slow evaporation technique. The growth conditions of the are studied confirmed powder X-ray diffraction studies. crystal was characterized using powdered XRD, FT-IR, UV–Vis–NIR, EDAX, TG–DTA. crystalline nature its various planes reflections observed XRD. presence functional groups FT-IR spectroscopic UV–Vis–NIR spectrum indicates that very absorption in entire visible near IR region suggesting suitability material for NLO applications. decomposition temperatures mass loss have estimated from thermogravimetric analysis.
springer.com
pubpeer.com参考文章(42)
Reema A. Porob, Sitara Z. Khan, S. C. Mojumdar, V. M. S. Verenkar, Synthesis,TG, DSC and infrared spectral study of NiMn2(C4H4O4)3·6N2H4 Journal of Thermal Analysis and Calorimetry. ,vol. 86, pp. 605- 608 ,(2006) , 10.1007/S10973-006-7715-Y
K. G. Varshney, A. Agrawal, S. C. Mojumdar, Pyridine based cerium(IV) phosphate hybrid fibrous ion exchanger Journal of Thermal Analysis and Calorimetry. ,vol. 90, pp. 731- 734 ,(2007) , 10.1007/S10973-007-8530-9
S. C. Mojumdar, C. Moresoli, L. C. Simon, R. L. Legge, Edible wheat gluten (WG) protein films Journal of Thermal Analysis and Calorimetry. ,vol. 104, pp. 929- 936 ,(2011) , 10.1007/S10973-011-1491-Z
S. Boomadevi, R. Dhanasekaran, P. Ramasamy, Investigations on Nucleation and Growth Kinetics of Urea Crystals from Methanol Crystal Research and Technology. ,vol. 37, pp. 159- 168 ,(2002) , 10.1002/1521-4079(200202)37:2/3<159::AID-CRAT159>3.0.CO;2-Y
M. Pajtášová, D. Ondrušová, E. Jóna, S. C. Mojumdar, S. L’alíková, T. Bazyláková, M. Gregor, Spectral and thermal characteristics of copper(II) carboxylates with fatty acid chains and their benzothiazole adducts Journal of Thermal Analysis and Calorimetry. ,vol. 100, pp. 769- 777 ,(2010) , 10.1007/S10973-010-0769-X
A.S Haja Hameed, G Ravi, R Dhanasekaran, P Ramasamy, Studies on organic indole-3-aldehyde single crystals Journal of Crystal Growth. ,vol. 212, pp. 227- 232 ,(2000) , 10.1016/S0022-0248(99)00896-9
G. Madhurambal, S. C. Mojumdar, S. Hariharan, P. Ramasamy, TG, DTA, FTIR and Raman spectral analysis of Zna/Mgb ammonium sulfate mixed crystals Journal of Thermal Analysis and Calorimetry. ,vol. 78, pp. 125- 133 ,(2004) , 10.1023/B:JTAN.0000042160.82063.C4
K. Moricová, E. Jóna, A. Plško, S. C. Mojumdar, Thermal stability of Li2O–SiO2–TiO2 gels evaluated by the induction period of crystallization Journal of Thermal Analysis and Calorimetry. ,vol. 100, pp. 817- 820 ,(2010) , 10.1007/S10973-010-0735-7
P. A. Angeli Mary, S. Dhanuskodi, Growth and characterization of a new nonlinear optical crystal : bis thiourea zinc chloride Crystal Research and Technology. ,vol. 36, pp. 1231- 1237 ,(2001) , 10.1002/1521-4079(200111)36:11<1231::AID-CRAT1231>3.0.CO;2-I
K. G. Varshney, A. Agrawal, S. C. Mojumdar, PECTIN BASED CERIUM (IV) AND THORIUM (IV) PHOSPHATES AS NOVEL HYBRID FIBROUS ION EXCHANGERS Synthesis, characterization and thermal behaviour Journal of Thermal Analysis and Calorimetry. ,vol. 81, pp. 183- 189 ,(2005) , 10.1007/S10973-005-0765-8