Three‐dimensional α colony characterization and prior‐β grain reconstruction of a lamellar Ti–6Al–4V specimen using near‐field high‐energy X‐ray diffraction microscopy

作者: E. Wielewski , D. B. Menasche , P. G. Callahan , R. M. Suter

DOI: 10.1107/S1600576715011139

关键词: MicrostructureX-ray crystallographyMolecular physicsLamellar structureNear and far fieldCrystallographyDiffractionMicroscopyMaterials scienceMisorientationCharacterization (materials science)

摘要: Near-field high energy X-ray diffraction microscopy (nf-HEDM) has been used to characterize the 3-D crystallographic orientation field of the hexagonal close-packed (hcp) α phase in a bulk Ti-6Al-4V specimen with lamellar (β-annealed) microstructure. These data have been segmented using misorientation-based grain finding algorithm, providing unprecedented information about complex morphologies and spatial misorientation distributions the transformed lamellae colonies. A Burgers relationship-based flood fill algorithm has implemented reconstruct orientations the high temperature body centred cubic (bcc) prior-β grains. The combination these has been gain understanding role structure on formation of specific observed transformed α colony structures. It is hoped that this can be develop transformation structures optimized for specific applications produce more physically realistic synthetic microstructures use simulations.

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