A simple route to disperse silver nanoparticles on the surfaces of silica nanofibers with excellent photocatalytic properties

作者: Xin Wang , Huiqing Fan , Pengrong Ren , Huawa Yu , Jin Li

DOI: 10.1016/J.MATERRESBULL.2012.03.042

关键词: NanofiberElectrospinningSilver nanoparticleMaterials scienceTransmission electron microscopyX-ray photoelectron spectroscopyMethyl orangeScanning electron microscopeChemical engineeringComposite numberNanotechnology

摘要: Abstract In this work, monodispersed silver nanoparticles decorated SiO 2 nanofibers were synthesized by electrospinning method, followed thermal treatment at 600 °C. Powder X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission (TEM), thermo-gravimetric analysis (TGA) and photoelectron spectroscopy (XPS) used to characterize the composite nanofibers. Accordingly, detailed formation mechanism of /Ag was discussed. Furthermore, an excellent catalytic activity fibers observed a degradation reaction methyl orange (MO) dye.

参考文章(33)
Joseph H. Flynn, Chapter 14 – Polymer degradation Handbook of Thermal Analysis and Calorimetry. ,vol. 3, pp. 587- 651 ,(2002) , 10.1016/S1573-4374(02)80017-6
Yongzhi Wang, Yaoxian Li, Songtao Yang, Guangliang Zhang, Dongmin An, Ce Wang, Qingbiao Yang, Xuesi Chen, Xiabin Jing, Yen Wei, A convenient route to polyvinyl pyrrolidone/silver nanocomposite by electrospinning Nanotechnology. ,vol. 17, pp. 3304- 3307 ,(2006) , 10.1088/0957-4484/17/13/037
Yugang Sun, Younan Xia, Shape-Controlled Synthesis of Gold and Silver Nanoparticles Science. ,vol. 298, pp. 2176- 2179 ,(2002) , 10.1126/SCIENCE.1077229
Wen-Ji Jin, Hwang Kyu Lee, Eun Hwan Jeong, Won Ho Park, Ji Ho Youk, Preparation of Polymer Nanofibers Containing Silver Nanoparticles by Using Poly(N-vinylpyrrolidone) Macromolecular Rapid Communications. ,vol. 26, pp. 1903- 1907 ,(2005) , 10.1002/MARC.200500569
G Mitrikas, C.C Trapalis, G Kordas, Tailoring the particle size of sol–gel derived silver nanoparticles in SiO2 Journal of Non-crystalline Solids. ,vol. 286, pp. 41- 50 ,(2001) , 10.1016/S0022-3093(01)00490-2
Xin Jiang, Shi Chen, Congwen Mao, Synthesis of Ag/SiO2 nanocomposite material by adsorption phase nanoreactor technique Colloids and Surfaces A: Physicochemical and Engineering Aspects. ,vol. 320, pp. 104- 110 ,(2008) , 10.1016/J.COLSURFA.2008.01.027
Jérôme Assal, Bengt Hallstedt, Ludwig J. Gauckler, Thermodynamic Assessment of the Silver–Oxygen System Journal of the American Ceramic Society. ,vol. 80, pp. 3054- 3060 ,(2005) , 10.1111/J.1151-2916.1997.TB03232.X
Ming Jin, Xintong Zhang, Shunsuke Nishimoto, Zhaoyue Liu, Donald A Tryk, Taketoshi Murakami, Akira Fujishima, Large-scale fabrication of Ag nanoparticles in PVP nanofibres and net-like silver nanofibre films by electrospinning Nanotechnology. ,vol. 18, pp. 075605- ,(2007) , 10.1088/0957-4484/18/7/075605
Dan Li, Jesse T. McCann, Matthew Gratt, Younan Xia, Photocatalytic deposition of gold nanoparticles on electrospun nanofibers of titania Chemical Physics Letters. ,vol. 394, pp. 387- 391 ,(2004) , 10.1016/J.CPLETT.2004.07.044
Minmin Teng, Hongtao Wang, Fengting Li, Bingru Zhang, Thioether-functionalized mesoporous fiber membranes: Sol–gel combined electrospun fabrication and their applications for Hg2+ removal Journal of Colloid and Interface Science. ,vol. 355, pp. 23- 28 ,(2011) , 10.1016/J.JCIS.2010.11.008