Novel TaPO5−xN2x/3 oxynitrides
作者： Erwan Ray , Franck Tessier , François Cheviré , Nathalie Herbert , Ronan Lebullenger
DOI: 10.1016/J.JALLCOM.2011.10.115
关键词: Analytical chemistry 、 BET theory 、 Spectrophotometry 、 Nitrogen 、 Ammonia 、 Inorganic chemistry 、 Solid solution 、 Nitriding 、 Thermal analysis 、 Amorphous solid 、 Materials science
摘要: Abstract A series of novel nitrided tantalophosphates has been prepared by nitridation X-ray amorphous TaPO 5 precursors under ammonia flow. By varying the temperature, 5− x N 2 /3 (1.6 g −1 , (ii) yellow to orange colors depending on nitrogen contents and (iii) formation a solid solution with variable oxygen contents. The corresponding oxynitrides have characterized several techniques including diffraction, oxygen/nitrogen elemental analyses, BET analysis, UV–vis spectrophotometry, thermal SEM, DRIFT NMR analyses.
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Roger Marchand, Wolfgang Schnick, Norbert Stock, Molecular, complex ionic, and solid state pon compounds Advances in Inorganic Chemistry. ,vol. 50, pp. 193- 233 ,(2000) , 10.1016/S0898-8838(00)50005-1
N. Fripiat, P. Grange, Influence of the nitridation parameters on the stoichiometry, structure and specific surface area of zirconium phosphate oxynitride catalysts Journal of Materials Science. ,vol. 34, pp. 2057- 2063 ,(1999) , 10.1023/A:1004551524765
J. Str�hle, Die Kristallstruktur des Tantal(V)‐nitrids Ta3N5 Zeitschrift für anorganische und allgemeine Chemie. ,vol. 402, pp. 47- 57 ,(1973) , 10.1002/ZAAC.19734020107
Franck TESSIER, Pascal MAILLARD, François CHEVIRÉ, Kazunari DOMEN, Shinichi KIKKAWA, Optical properties of oxynitride powders Journal of the Ceramic Society of Japan. ,vol. 117, pp. 1- 5 ,(2009) , 10.2109/JCERSJ2.117.1
Wolfgang Gruner, Birgit Wollein, Walter Lengauer, ɛ-TaN as a Reference Material for the Determination of High Nitrogen Contents Mikrochimica Acta. ,vol. 146, pp. 1- 6 ,(2004) , 10.1007/S00604-003-0169-Z
K. S. W. Sing, Reporting physisorption data for gas/solid systems with special reference to the determination of surface area and porosity (Recommendations 1984) Pure and Applied Chemistry. ,vol. 57, pp. 603- 619 ,(1985) , 10.1351/PAC198557040603
J.J. Benı́tez, A. Dı́az, Y. Laurent, J.A. Odriozola, Characterisation, surface hydrolysis and nitrogen stability in aluminophosphate oxynitride (AlPON) catalysts Applied Catalysis A-general. ,vol. 176, pp. 177- 187 ,(1999) , 10.1016/S0926-860X(98)00241-5
V Peltier, R Conanec, R Marchand, Y Laurent, S Delsarte, E Gueguen, P Grange, A novel family of mixed gallium aluminum phosphorus oxynitrides: their synthesis, characterization and utilization in heterogeneous catalysis Materials Science and Engineering B-advanced Functional Solid-state Materials. ,vol. 47, pp. 177- 183 ,(1997) , 10.1016/S0921-5107(97)00026-3
A. Dı́az, J.J. Benı́tez, Y. Laurent, J.A. Odriozola, Diffuse reflectance infrared spectra and their relation to the thermal stability of aluminophosphate oxynitrides as a function of nitrogen content Journal of Non-crystalline Solids. ,vol. 238, pp. 163- 170 ,(1998) , 10.1016/S0022-3093(98)00677-2
G.T. Stranford, R.A. Condrate, A vibrational spectral study of hydrated tantalum phosphate (TaPO5) phases Journal of Solid State Chemistry. ,vol. 85, pp. 326- 331 ,(1990) , 10.1016/S0022-4596(05)80091-X