Controlling the crystallisation of oxide materials by solvothermal chemistry: tuning composition, substitution and morphology of functional solids
作者： Craig I. Hiley , Richard I. Walton
DOI: 10.1039/C6CE01655C
关键词: Nanotechnology 、 Crystallite 、 Bismuth 、 Crystallization 、 Solvothermal synthesis 、 Chemistry 、 Particle 、 Ternary operation 、 Oxide 、 Chemical composition
摘要: We provide an overview of currently emerging areas in the solvothermal synthesis polycrystalline oxide materials that illustrate how tailoring may be possible to target formation functional solids. various levels control preparation oxides with interesting structures and compositions by choosing examples three aspects recent chemistry: (1) discovery, (2) substitutional chemistry (3) adjustment crystal morphology size. This includes new ruthenium, iridium bismuth, novel CeO2 TiO2, form binary ternary oxides. The accumulated research illustrates potential for fine properties targeted crystallisation solid selected chemical composition particle shape dimensions from nanoscale micronscale. These benefits uniquely arise variation use solution-mediated crystallisation. conclude discussing future work must focus on developing predictive synthesis, where conditions could design a material desired properties.
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