Mn3O4 Nanoparticle Synthesis via Ionic Liquid-Assisted Route
作者： M. Ramalakshmi , P. Shakkthivel , Min Kim
DOI: 10.1007/S10948-014-2613-1
关键词: Fourier transform infrared spectroscopy 、 Thermogravimetric analysis 、 Materials science 、 Phase (matter) 、 Sulfonate 、 Nuclear magnetic resonance 、 Nanocrystal 、 Chemical engineering 、 Nanoparticle 、 Ionic liquid 、 Superparamagnetism
摘要: Via the green chemistry route, a new class of Mn3O4 nanoparticles has been synthesized using 1-n-butyl-3-methylimidazolium trifluoromethane sulfonate [BMIM][TfO] ionic liquid, which serves as capping agent. The thermal behavior, phase structure, morphology, and magnetic properties samples are characterized by thermogravimetric analysis (TGA), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), Field emission scanning electron microscopy (FE-SEM), Vibrating sample magnetometer (VSM) studies. phase-pure nanocrystals with 40-nm narrow particle size distribution obtained significant influence liquid. show superparamagnetic behavior.
springer.com
sci-hub.se 参考文章(20)
Kazuo Nakamoto, Infrared and Raman Spectra of Inorganic and Coordination Compounds ,(1978)
Shuijin Lei, Kaibin Tang, Zhen Fang, Huagui Zheng, Ultrasonic-Assisted Synthesis of Colloidal Mn3O4 Nanoparticles at Normal Temperature and Pressure Crystal Growth & Design. ,vol. 6, pp. 1757- 1760 ,(2006) , 10.1021/CG050402O
T Ozkaya, Abdulhadi Baykal, HÜSEYİN Kavas, Yüksel Köseoğlu, Muhammet S Toprak, A novel synthetic route to Mn3O4 nanoparticles and their magnetic evaluation Physica B-condensed Matter. ,vol. 403, pp. 3760- 3764 ,(2008) , 10.1016/J.PHYSB.2008.07.002
D.P. Dubal, D.S. Dhawale, R.R. Salunkhe, S.M. Pawar, C.D. Lokhande, A novel chemical synthesis and characterization of Mn3O4 thin films for supercapacitor application Applied Surface Science. ,vol. 256, pp. 4411- 4416 ,(2010) , 10.1016/J.APSUSC.2009.12.057
Tatsuji Yamashita, Albert Vannice, NO Decomposition over Mn2O3and Mn3O4 Journal of Catalysis. ,vol. 163, pp. 158- 168 ,(1996) , 10.1006/JCAT.1996.0315
Jianmin Ma, Jiabiao Lian, Xiaochuan Duan, Zhifang Liu, Peng Peng, Xiaodi Liu, Tongil Kim, Wenjun Zheng, Growth of tellurium nanowire bundles from an ionic liquid precursor CrystEngComm. ,vol. 13, pp. 2774- 2778 ,(2011) , 10.1039/C0CE00978D
Jairton Dupont, Gledison S. Fonseca, Alexandre P. Umpierre, Paulo F. P. Fichtner, Sergio R. Teixeira, Transition-Metal Nanoparticles in Imidazolium Ionic Liquids: Recycable Catalysts for Biphasic Hydrogenation Reactions Journal of the American Chemical Society. ,vol. 124, pp. 4228- 4229 ,(2002) , 10.1021/JA025818U
Jairton Dupont, Roberto F. de Souza, Paulo A. Z. Suarez, Ionic liquid (molten salt) phase organometallic catalysis. Chemical Reviews. ,vol. 102, pp. 3667- 3692 ,(2002) , 10.1021/CR010338R
YQ Chang, XY Xu, XH Luo, CP Chen, DP Yu, None, Synthesis and characterization of Mn3O4 nanoparticles Journal of Crystal Growth. ,vol. 264, pp. 232- 236 ,(2004) , 10.1016/J.JCRYSGRO.2003.11.117
E.R. Stobbe, B.A. de Boer, J.W. Geus, The reduction and oxidation behaviour of manganese oxides Catalysis Today. ,vol. 47, pp. 161- 167 ,(1999) , 10.1016/S0920-5861(98)00296-X