Quantification of corticosteroids in human plasma by liquid chromatography-thermospray mass spectrometry using stable isotope dilution
作者： Hiromi Shibasaki , Takashi Furuta , Yasuji Kasuya
DOI: 10.1016/S0378-4347(96)00489-6
关键词: Quantitative analysis (chemistry) 、 High-performance liquid chromatography 、 Cortisone 、 Chromatography 、 Elution 、 Chemistry 、 Isotope dilution 、 Thermospray 、 Mass spectrometry 、 Ammonium
摘要: … using 0.05 M ammonium formate–acetonitrile (65:35, v/v) permitted accurate quantification … linear fitting of the peak-area ratios versus the mixed molar ratios of cortisol/cortisol-d 5 , …
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sci-hub.se 参考文章(23)
Nobuo Tanaka, Edward R. Thornton, Isotope effects in hydrophobic binding measured by high-pressure liquid chromatography Journal of the American Chemical Society. ,vol. 98, pp. 1617- 1619 ,(1976) , 10.1021/JA00422A076
M Hariharan, S Naga, T VanNoord, E K Kindt, Simultaneous assay of corticosterone and cortisol in plasma by reversed-phase liquid chromatography. Clinical Chemistry. ,vol. 38, pp. 346- 352 ,(1992) , 10.1093/CLINCHEM/38.3.346
Simon J. Gaskell, Keith Rollins, Richard W. Smith, Carol E. Parker, Determination of serum cortisol by thermospray liquid chromatography/mass spectrometry: comparison with gas chromatography/mass spectrometry. Journal of Mass Spectrometry. ,vol. 14, pp. 717- 722 ,(1987) , 10.1002/BMS.1200141205
AM Jeffrey, PP Fu, None, Isotopic separations of tritium-substituted compounds from protium analogues by high-pressure liquid chromatography. Analytical Biochemistry. ,vol. 77, pp. 298- 302 ,(1977) , 10.1016/0003-2697(77)90318-9
Hiromi Shibasaki, Takashi Furuta, Yasuji Kasuya, Stable isotope dilution mass spectrometry for the simultaneous determination of cortisol, cortisone, prednisolone and prednisone in plasma Journal of Chromatography B: Biomedical Sciences and Applications. ,vol. 579, pp. 193- 202 ,(1992) , 10.1016/0378-4347(92)80382-Z
D. Watson, G. W. Taylor, S. Murray, Steroid glucronide conjugates: Analysis by thermospray liquid chromatography negative ion mass spectrometry Biological Mass Spectrometry. ,vol. 13, pp. 65- 69 ,(1986) , 10.1002/BMS.1200130204
Nora V. Esteban, Alfred L. Yergey, Daniel J. Liberato, Therese Loughlin, D. Lynn Loriaux, Stable isotope dilution method using thermospray liquid chromatography/mass spectrometry for quantification of daily cortisol production in humans Journal of Mass Spectrometry. ,vol. 15, pp. 603- 608 ,(1988) , 10.1002/BMS.1200151105
Nora V. Esteban, Alfred L. Yergey, Cortisol production rates measured by liquid chromatography/mass spectrometry. Steroids. ,vol. 55, pp. 152- 158 ,(1990) , 10.1016/0039-128X(90)90103-I
M.S. Lant, L.E. Martin, J. Oxford, Qualitative and Quantitative Analysis of Ranitidine and Its Metabolites by High-Performance Liquid Chromatography-Mass Spectrometry Journal of Chromatography A. ,vol. 323, pp. 143- 152 ,(1985) , 10.1016/S0021-9673(01)90379-6
Crist N. Filer, Robert Fazio, David G. Ahern, (.+-.)-[Methyl-3H and -2H]mianserin. Participants in a dramatic instance of HPLC isotopic fractionation The Journal of Organic Chemistry. ,vol. 46, pp. 3344- 3346 ,(1981) , 10.1021/JO00329A043