Synthesis and Characterization of a New Difunctional Ligand and Its Metal Complexes: An Experimental, Theoretical, Cyclic Voltammetric, and Antimicrobial Study
作者： Haci Baykara , Salih Ilhan , Abdussamet Oztomsuk , M. Salih Seyitoglu , Abdulkadir Levent
DOI: 10.1080/15533174.2013.872134
关键词: Chelation 、 Cyclic voltammetry 、 Molar conductivity 、 Inorganic chemistry 、 Redox 、 Metal 、 Ligand 、 Thermogravimetric analysis 、 Chemistry 、 Schiff base
摘要: A new difunctional Schiff base ligand and its some metal complexes were synthesized. The compounds characterized by elemental analysis, 1H-NMR, 13C-NMR, FT-IR, UV-VIS, magnetic susceptibility measurements, molar conductivity thermal gravimetric analysis techniques. Additionally, DPPH scavenging, chelating antibacterial activity of examined via in vitro methods. lowest scavenging observed Co(II) as 36.28% highest was 52.00%. cyclic voltammetric study also carried out to determine redox potentials the compounds. Some theoretical studies such HOMO-LUMO, mapped electron density successfully.
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