Dereplication of antioxidant compounds in Bene (Pistacia atlantica subsp. mutica) hull using a multiplex approach of HPLC-DAD, LC-MS and (1)H NMR techniques.
作者： Mitra Rezaie , Reza Farhoosh , Ngoc Pham , Ronald J. Quinn , Mehrdad Iranshahi
DOI: 10.1016/J.JPBA.2015.09.005
关键词: Pistacia 、 Rutin 、 Liquid chromatography–mass spectrometry 、 Chromatography 、 DPPH 、 Caffeic acid 、 Pistacia atlantica 、 Chemistry 、 Quercetin 、 Gallic acid
摘要: Bene is an edible fruit from the tree Pistacia atlantica subsp. mutica, and of steadily growing interest in recent years due to its significant antioxidant properties potential health benefits. An activity-guided fractionation methanol extract hull together with integrated approach HPLC-DAD, LC-MS (1)H NMR techniques led identification main phenolic compounds for first time. Radical scavenging activity each fraction/compound was tested using DPPH FRAP assays. The content fractions also determined by Folin-Ciocalteu's method. identified were luteolin (46.53% w/w total extract), gallic acid (9.84% w/w), 2″-O-galloylisoquercitrin (0.53% quercetin 3-rutinoside (0.34% w/w) 2″-O-cis-caffeoylquercitrin (0.26% w/w). minor liquid chromatography-positive/negative electrospray ionization tandem mass spectrometry. structure-antioxidant relationship phenolics are discussed this paper.
core.ac.uk
um.ac.ir
elsevier.com
sci-hub.se 参考文章(25)
Vernon L. Singleton, Rudolf Orthofer, Rosa M. Lamuela-Raventós, ANALYSIS OF TOTAL PHENOLS AND OTHER OXIDATION SUBSTRATES AND ANTIOXIDANTS BY MEANS OF FOLIN-CIOCALTEU REAGENT Methods in Enzymology. ,vol. 299, pp. 152- 178 ,(1999) , 10.1016/S0076-6879(99)99017-1
Riccardo Amorati, Luca Valgimigli, Modulation of the antioxidant activity of phenols by non-covalent interactions Organic and Biomolecular Chemistry. ,vol. 10, pp. 4147- 4158 ,(2012) , 10.1039/C2OB25174D
Qing-An Zhang, Xue-Hui Fan, Zhi-Qi Zhang, Tao Li, Cai-Ping Zhu, Xiao-Rui Zhang, Wei Song, Extraction, antioxidant capacity and identification of Semen Astragali Complanati (Astragalus complanatus R. Br.) phenolics. Food Chemistry. ,vol. 141, pp. 1295- 1300 ,(2013) , 10.1016/J.FOODCHEM.2013.04.014
Pradeep Pratap Singh, Ambika, S.M.S. Chauhan, Activity guided isolation of antioxidants from the leaves of Ricinus communis L. Food Chemistry. ,vol. 114, pp. 1069- 1072 ,(2009) , 10.1016/J.FOODCHEM.2008.10.020
Mitra Rezaie, Reza Farhoosh, Mehrdad Iranshahi, Ali Sharif, Shiva Golmohamadzadeh, Ultrasonic-assisted extraction of antioxidative compounds from Bene (Pistacia atlantica subsp. mutica) hull using various solvents of different physicochemical properties. Food Chemistry. ,vol. 173, pp. 577- 583 ,(2015) , 10.1016/J.FOODCHEM.2014.10.081
Shaida Fariza Sulaiman, Azliana Abu Bakar Sajak, Kheng Leong Ooi, Supriatno, Eng Meng Seow, Effect of solvents in extracting polyphenols and antioxidants of selected raw vegetables Journal of Food Composition and Analysis. ,vol. 24, pp. 506- 515 ,(2011) , 10.1016/J.JFCA.2011.01.020
A. Kumaran, R. Joel Karunakaran, Activity-guided isolation and identification of free radical-scavenging components from an aqueous extract of Coleus aromaticus Food Chemistry. ,vol. 100, pp. 356- 361 ,(2007) , 10.1016/J.FOODCHEM.2005.09.051
Daniel Rösch, Meike Bergmann, Dietrich Knorr, Lothar W. Kroh, Structure−Antioxidant Efficiency Relationships of Phenolic Compounds and Their Contribution to the Antioxidant Activity of Sea Buckthorn Juice Journal of Agricultural and Food Chemistry. ,vol. 51, pp. 4233- 4239 ,(2003) , 10.1021/JF0300339
Patrick Trouillas, Philippe Marsal, Didier Siri, Roberto Lazzaroni, Jean-Luc Duroux, A DFT study of the reactivity of OH groups in quercetin and taxifolin antioxidants : The specificity of the 3-OH site Food Chemistry. ,vol. 97, pp. 679- 688 ,(2006) , 10.1016/J.FOODCHEM.2005.05.042
Reza Farhoosh, Mohammad Hossein Tavassoli-Kafrani, Ali Sharif, Antioxidant activity of sesame, rice bran and bene hull oils and their unsaponifiable matters European Journal of Lipid Science and Technology. ,vol. 113, pp. 506- 512 ,(2011) , 10.1002/EJLT.201000402