Synthesis of zinc oxide nanocrystals by thermal decomposition of Zn-oleate in organic medium
作者： ChenSha Li , YuNing Li , YiLiang Wu , Beng S. Ong , Rafik O. Loutfy
DOI: 10.1007/S11431-008-0236-0
关键词: Crystallinity 、 Chemical engineering 、 Boiling point 、 Thermal decomposition 、 Reagent 、 Materials science 、 Zinc nitrate 、 Nanocrystal 、 Zinc 、 Octadecene 、 Inorganic chemistry 、 General Engineering 、 General Materials Science
摘要: We report the synthesis of uniform-sized hexagonal ZnO nanocrystals by thermolysis Zn-oleate complex, which was prepared from reaction inexpensive and environmentally friendly reagents such as zinc nitrate sodium oleate. Two organic compounds with different boiling points, octadecene octylether, were selected medium for complex. Under optimized conditions, we able to synthesize nanoparticles size being about 10 nm. X-ray diffraction transmission electron micrograph (TEM) images confirmed high crystallinity nanocrystals.
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