Temperature dependence of fracture toughness of silica/epoxy composites: Related to microstructure of nano- and micro-particles packing
作者： Soon-Chul Kwon , Tadaharu Adachi , Wakako Araki
DOI: 10.1016/J.COMPOSITESB.2007.10.008
关键词: Volume fraction 、 Fracture toughness 、 Nanocomposite 、 Materials science 、 Microstructure 、 Composite material 、 Concentration effect 、 Nano- 、 Particle size 、 Epoxy
摘要: Abstract Temperature dependence of the fracture toughness epoxy composites reinforced with nano- and micro-silica particles was evaluated. Epoxy containing varied composition ratios ΦSP spherical particles, 240 nm 1.56 μm, were prepared at a fixed volume fraction (VP = 0.30). The thermo-viscoelasticity neat measured 143 K, 185 K, 228 K, 296 K, 363 K, 399 K. Experimental results revealed that strongly depended on microstructure micro-particles bidispersion as well its interactions matrix all temperature, but toughened due to increase in mobility relaxation temperatures.
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sci-hub.se 参考文章(16)
J. P. Benthem, W. T. Koiter, Asymptotic approximations to crack problems Springer, Dordrecht. pp. 131- 178 ,(1973) , 10.1007/978-94-017-2260-5_3
Robert F. Landel, Lawrence E. Nielsen, Mechanical Properties of Polymers and Composites ,(1993)
J. Spanoudakis, R. J. Young, Crack propagation in a glass particle-filled epoxy resin Journal of Materials Science. ,vol. 19, pp. 487- 496 ,(1984) , 10.1007/BF02403235
S KWON, T ADACHI, W ARAKI, A YAMAJI, Thermo-viscoelastic properties of silica particulate-reinforced epoxy composites : Considered in terms of the particle packing model Acta Materialia. ,vol. 54, pp. 3369- 3374 ,(2006) , 10.1016/J.ACTAMAT.2006.03.026
R. Kitey, H.V. Tippur, Dynamic crack growth in particulate bimaterials having discrete and diffuse interfaces: Role of microstructure Engineering Fracture Mechanics. ,vol. 72, pp. 2721- 2743 ,(2005) , 10.1016/J.ENGFRACMECH.2005.07.006
R.J. Butcher, C.-E. Rousseau, H.V. Tippur, A functionally graded particulate composite: Preparation, measurements and failure analysis Acta Materialia. ,vol. 47, pp. 259- 268 ,(1998) , 10.1016/S1359-6454(98)00305-X
A. C. Moloney, H. H. Kausch, T. Kaiser, H. R. Beer, Parameters determining the strength and toughness of particulate filled epoxide resins Journal of Materials Science. ,vol. 22, pp. 381- 393 ,(1987) , 10.1007/BF01160743
Soon Chul Kwon, Tadaharu Adachi, Wakako Araki, Akihiko Yamaji, Effect of Particle Size on Fracture Toughness of Spherical-Silica Particle Filled Epoxy Composites Key Engineering Materials. pp. 207- 212 ,(2005) , 10.4028/WWW.SCIENTIFIC.NET/KEM.297-300.207
Lawrence E. Nielsen, Cross-Linking–Effect on Physical Properties of Polymers Journal of Macromolecular Science, Part C. ,vol. 3, pp. 69- 103 ,(1969) , 10.1080/15583726908545897
Soon-Chul Kwon, Tadaharu Adachi, Strength and fracture toughness of nano and micron-silica particles bidispersed epoxy composites: evaluated by fragility parameter Journal of Materials Science. ,vol. 42, pp. 5516- 5523 ,(2007) , 10.1007/S10853-006-1025-4