Damage and deuterium trapping in highly‐oriented pyrolytic graphite

作者: R. Siegele , J. Roth , B. M. U. Scherzer , S. J. Pennycook

DOI: 10.1063/1.353126

关键词: Atomic physicsTransmission electron microscopyChemistryNuclear reaction analysisFluenceRange (particle radiation)Ion implantationDeuteriumAnalytical chemistryPyrolytic carbonHighly oriented pyrolytic graphite

摘要: In this work the buildup of damage due to deuterium implantation in highly‐oriented pyrolytic graphite (HOPG) is investigated. HOPG was implanted with 10–30 keV D3+ at different target temperatures between room temperature and 773 K fluences from 1014 1018 D/cm2. Subsequently, retained were measured by Rutherford backscattering (RBS) a channeling direction (RBSc) D(3He, p)α nuclear reaction analysis (NRA), respectively. The selected samples additionally observed transmission electron microscopy (TEM). initial trapping efficiency unity whole energy range. maximum retention deuterium, however, depends on energy. RBSc starts saturate 5×1015 D/cm2 (295 K) 1.3×1017 (773 K). Both are well below fluence which amorphization TEM.

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