Structural Analysis of Carboxylic Acid-functionalized Multi-walled Carbon Nanotubes
作者：
DOI: 10.4313/JKEM.2007.20.10.878
关键词: Carbon nanotube 、 Aqueous solution 、 Materials science 、 Carboxylic acid 、 Surface modification 、 Thermal stability 、 Thermogravimetric analysis 、 Fourier transform infrared spectroscopy 、 Organic chemistry 、 Carboxylation 、 Chemical engineering
摘要: Carboxylated multi-walled carbon nanotubes (MWNTs) were in detail characterized by XRD, XPS, FTIR, and thermogravimetric measurements. Carboxylic acid groups functionalized to MWNTs under aqueous condition. The changes of sonication reflux conditions rarely influenced the degree carboxylation on MWNTs, but decreased thermal stability resultant carboxylated MWNTs. XRD results showed that diffraction peaks (100), (101), (102) pristine disappeared after treatment, peak (002) was Preserved introduction carboxylic caused improve dispersibility water.
koreascience.or.kr参考文章(15)
D. Reznik, C. H. Olk, D. A. Neumann, J. R. D. Copley, X-ray powder diffraction from carbon nanotubes and nanoparticles Physical Review B. ,vol. 52, pp. 116- 124 ,(1995) , 10.1103/PHYSREVB.52.116
Geon-Woong Lee, Satish Kumar, Dispersion of Nitric Acid-Treated SWNTs in Organic Solvents and Solvent Mixtures Journal of Physical Chemistry B. ,vol. 109, pp. 17128- 17133 ,(2005) , 10.1021/JP052943U
Shoushan Fan, Michael G Chapline, Nathan R Franklin, Thomas W Tombler, Alan M Cassell, Hongjie Dai, Self-Oriented Regular Arrays of Carbon Nanotubes and Their Field Emission Properties Science. ,vol. 283, pp. 512- 514 ,(1999) , 10.1126/SCIENCE.283.5401.512
A. Thess, R. Lee, P. Nikolaev, H. Dai, P. Petit, J. Robert, C. Xu, Y. H. Lee, S. G. Kim, A. G. Rinzler, D. T. Colbert, G. E. Scuseria, D. Tomanek, J. E. Fischer, R. E. Smalley, Crystalline Ropes of Metallic Carbon Nanotubes Science. ,vol. 273, pp. 483- 487 ,(1996) , 10.1126/SCIENCE.273.5274.483
Christopher A. Dyke, James M. Tour, Overcoming the Insolubility of Carbon Nanotubes Through High Degrees of Sidewall Functionalization Chemistry: A European Journal. ,vol. 10, pp. 812- 817 ,(2004) , 10.1002/CHEM.200305534
Anyuan Cao, Hongwei Zhu, Xianfeng Zhang, Xuesong Li, Dianbo Ruan, Cailu Xu, Binqing Wei, Ji Liang, Dehai Wu, Hydrogen storage of dense-aligned carbon nanotubes Chemical Physics Letters. ,vol. 342, pp. 510- 514 ,(2001) , 10.1016/S0009-2614(01)00619-4
Jian Chen, Mark A Hamon, Hui Hu, Yongsheng Chen, Apparao M Rao, Peter C Eklund, Robert C Haddon, Solution Properties of Single-Walled Carbon Nanotubes Science. ,vol. 282, pp. 95- 98 ,(1998) , 10.1126/SCIENCE.282.5386.95
Q. Cao, S.-H. Hur, Z.-T. Zhu, Y. G. Sun, C.-J. Wang, M. A. Meitl, M. Shim, J. A. Rogers, Highly bendable, transparent thin-film transistors that use carbon-nanotube-based conductors and semiconductors with elastomeric dielectrics Advanced Materials. ,vol. 18, pp. 304- 309 ,(2006) , 10.1002/ADMA.200501740
Hui-Wen Chen, Ren-Jang Wu, Kuo-Hung Chan, Yih-Lu Sun, Pi-Guey Su, The application of CNT/Nafion composite material to low humidity sensing measurement Sensors and Actuators B-chemical. ,vol. 104, pp. 80- 84 ,(2005) , 10.1016/J.SNB.2004.04.105
Yutaka Maniwa, Ryuji Fujiwara, Hiroshi Kira, Hideki Tou, Eiji Nishibori, Masaki Takata, Makoto Sakata, Akihiko Fujiwara, Xinluo Zhao, Sumio Iijima, Yoshinori Ando, Multiwalled carbon nanotubes grown in hydrogen atmosphere : An x-ray diffraction study Physical Review B. ,vol. 64, pp. 073105- ,(2001) , 10.1103/PHYSREVB.64.073105