Studies in starch structure. I.—analytical methods†

作者: C. H. F. Fuller , L. H. Lampitt , L. Coton

DOI: 10.1002/JSFA.2740061103

关键词: Serial dilutionBoiling tubeViscosityStarchHomogeneousDegradation (geology)ChemistryHydrolysateHydrolysisChromatography

摘要: In order to characterize starch fractions which cannot be prepared in the form of homogeneous dry powders without degradation, scheme analysis has been modified so as avoid working on a previously-dried substance. A semi-micro method for determination concentration solutions is described hydrolysed and reducing power neutralized hydrolysate determined transfer from single boiling tube. Modifications power, limiting viscosity number, properties polysaccharide-iodine complex limit conversion by β-amylase permit these characteristics using dilutions solution known concentration. Adoption methods leads greater precision net saving time.

参考文章(7)
S Dayton, S Seifter, The estimation of glycogen with the anthrone reagent Archives of Biochemistry and Biophysics. ,vol. 25, pp. 191- 200 ,(1950)
W. Z. Hassid, Determination of Sugars in Plants Industrial & Engineering Chemistry Analytical Edition. ,vol. 9, pp. 228- 229 ,(1937) , 10.1021/AC50109A015
L. H. Lampitt, C. H. F. Fuller, N. Goldenberg, The fractionation of wheat starch. II. The reducing powers of starch fractions Journal of the Society of Chemical Industry. ,vol. 60, pp. 25- 29 ,(1941) , 10.1002/JCTB.5000600201
Sylvia. Lansky, Mary. Kooi, Thomas John. Schoch, Properties of the Fractions and Linear Subfractions from Various Starches Journal of the American Chemical Society. ,vol. 71, pp. 4066- 4075 ,(1949) , 10.1021/JA01180A056
L. Coton, L. H. Lampitt, C. H. F. Fuller, Studies in starch structure. II.—the determination of iodine absorption by amperometric titration Journal of the Science of Food and Agriculture. ,vol. 6, pp. 660- 664 ,(1955) , 10.1002/JSFA.2740061104
S. J. Pirt, W. J. Whelan, The determination of starch by acid hydrolysis. Journal of the Science of Food and Agriculture. ,vol. 2, pp. 224- 228 ,(1951) , 10.1002/JSFA.2740020507
Laetta J. Gundrum, C. E. Rist, Ivan A. Wolff, A Simplified Procedure for the Characterization of Starch Fractions by Viscosity and Iodine Sorption Journal of the American Chemical Society. ,vol. 72, pp. 5188- 5191 ,(1950) , 10.1021/JA01167A111