Synthesis and Characterization of Nano-Hexaferrites SrFe12O19 by Aqueous Solution Method

作者: Jian An Liu , Mei Mei Zhang , Yan Fei Zhang , Shu Jiang Liu

DOI: 10.4028/WWW.SCIENTIFIC.NET/AMR.306-307.404

关键词: Materials scienceMagnetometerAnalytical chemistryTransmission electron microscopyCoercivityNanometreNano-DiffractionFourier transform infrared spectroscopyAqueous solutionGeneral Engineering

摘要: Nano-hexaferrite SrFe12O19 has been prepared using the aqueous solution method. The structure and magnetic properties of SrFe12O19 have systematically been investigated by X-ray diffraction (XRD), Thermo gravimetric (TG), Fourier transform infrared spectroscopy (FTIR), Transmission Electron Microscopy (TEM), as well as Vibrating Sample Magnetometer (VSM). The XRD and TEM results showed that the samples are composed of SrFe12O19 nano-particles which are on average 70×50nm in dimensions when treated at 1200°C for 2 hours. The magnetic properties indicated that the saturation magnetization and the intrinsic coercivity were 48 Am2/kg and 506KA/m, respectively. The aqueous solution method is generally applicable to produce the nano-hexaferrite SrFe12O19 and is proved to be a promising method for fast synthesis of nanometer materials using nitrate.

参考文章(5)
D. D. Zaitsev, E. A. Gravchikova, P. E. Kazin, A. V. Garshev, Yu. D. Tret’yakov, M. Jansen, Preparation of magnetic glass-ceramics through glass crystallization in the Na2O-SrO-Fe2O3-B2O3 system Inorganic Materials. ,vol. 42, pp. 326- 330 ,(2006) , 10.1134/S0020168506030198
D.D. Zaitsev, P.E. Kazin, L.A. Trusov, D.A. Vishnyakov, Yu.D. Tretyakov, M. Jansen, Synthesis of magnetic glass-ceramics in the system SrO–Fe2O3–Al2O3–B2O3 Journal of Magnetism and Magnetic Materials. ,vol. 300, pp. 473- 475 ,(2006) , 10.1016/J.JMMM.2005.10.197
Dmitry D. Zaitsev, Ekaterina A. Gravchikova, Pavel E. Kazin, Yury D. Tretyakov, Martin Jansen, Glass–Ceramic Composites with Strontium Hexaferrite Ultrafine Particles in the SrO–Fe2O3–B2O3–SiO2 System International Journal of Applied Ceramic Technology. ,vol. 3, pp. 279- 283 ,(2006) , 10.1111/J.1744-7402.2006.02093.X
Zai-Bing Guo, Wei-Ping Ding, Wei Zhong, Jian-Rong Zhang, You-Wei Du, Preparation and magnetic properties of SrFe12O19 particles prepared by the salt-melt method Journal of Magnetism and Magnetic Materials. ,vol. 175, pp. 333- 336 ,(1997) , 10.1016/S0304-8853(97)00206-0