Comparison of four extraction/methylation analytical methods to measure fatty acid composition by gas chromatography in meat

作者: M. Juárez , O. Polvillo , M. Contò , A. Ficco , S. Ballico

DOI: 10.1016/J.CHROMA.2008.03.004

关键词: Fatty acid methyl esterSaponificationFatty acidRepeatabilityExtraction (chemistry)ChemistryChromatographyDerivatizationReproducibilityPolyunsaturated fatty acid

摘要: … values, except for the polyunsaturated fatty acids, showing higher variation than the former … the saponification method would be more convenient for polyunsaturated fatty acid analysis, …

参考文章(33)
Jan Fritsche, Sonja Fritsche, M. B. Solomon, M. M. Mossoba, M. P. Yurawecz, K. Morehouse, Y. Ku, Quantitative determination of conjugated linoleic acid isomers in beef fat European Journal of Lipid Science and Technology. ,vol. 102, pp. 667- 672 ,(2000) , 10.1002/1438-9312(200011)102:11<667::AID-EJLT667>3.0.CO;2-N
Najibullah Sehat, Martin P. Yurawecz, John A. G. Roach, Magdi M. Mossoba, John K. G. Kramer, Youh Ku, Silver‐ion high‐performance liquid chromatographic separation and identification of conjugated linoleic acid isomers Lipids. ,vol. 33, pp. 217- 221 ,(1998) , 10.1007/S11745-998-0198-6
G.J. Haan, S. Van Der Heide, B.G. Wolthers, Analysis of fatty acids from human lipids by gas chromatography Journal of Chromatography A. ,vol. 162, pp. 261- 271 ,(1979) , 10.1016/S0378-4347(00)81513-3
L. D. Metcalfe, A. A. Schmitz, J. R. Pelka, Rapid Preparation of Fatty Acid Esters from Lipids for Gas Chromatographic Analysis. Analytical Chemistry. ,vol. 38, pp. 514- 515 ,(1966) , 10.1021/AC60235A044
R. G. Ackman, Losses of DHA from high temperatures of columns during GLC of methyl esters of long-chain omega-3 fatty acids Journal of the American Oil Chemists' Society. ,vol. 83, pp. 1069- 1070 ,(2006) , 10.1007/S11746-006-5164-1
J.D. Wood, M. Enser, A.V. Fisher, G.R. Nute, P.R. Sheard, R.I. Richardson, S.I. Hughes, F.M. Whittington, Fat deposition, fatty acid composition and meat quality: A review Meat Science. ,vol. 78, pp. 343- 358 ,(2008) , 10.1016/J.MEATSCI.2007.07.019
Yeonhwa Park, Karen J. Albright, Zu Y. Cai, Michael W. Pariza, Comparison of Methylation Procedures for Conjugated Linoleic Acid and Artifact Formation by Commercial (Trimethylsilyl)diazomethane Journal of Agricultural and Food Chemistry. ,vol. 49, pp. 1158- 1164 ,(2001) , 10.1021/JF001209Z
Dirk Dannenberger, Gerd Nuernberg, Nigel Scollan, Klaus Ender, Karin Nuernberg, Diet alters the fatty acid composition of individual phospholipid classes in beef muscle. Journal of Agricultural and Food Chemistry. ,vol. 55, pp. 452- 460 ,(2007) , 10.1021/JF061793X
Noelia Aldai, Brendan E Murray, Ana I Nájera, Declan J Troy, Koldo Osoro, Derivatization of fatty acids and its application for conjugated linoleic acid studies in ruminant meat lipids Journal of the Science of Food and Agriculture. ,vol. 85, pp. 1073- 1083 ,(2005) , 10.1002/JSFA.2110