Extracting grain-orientation-dependent data from in situ time-of-flight neutron diffraction. I. Inverse pole figures

作者: G. M. Stoica , A. D. Stoica , K. An , D. Ma , S. C. Vogel

DOI: 10.1107/S1600576714023036

关键词: OpticsNormalization (statistics)DiffractometerPhysicsSpallation Neutron SourceInverseNeutron diffractionWeightingTime of flightComputational physicsPole figure

摘要: The problem of calculating the inverse pole figure (IPF) is analyzed from perspective application time-of flight neutron diffraction toin situmonitoring thermomechanical behavior engineering materials. On basis a quasi-Monte Carlo (QMC) method, consistent set grain orientations generated and used to compute weighting factors for IPF normalization. are instrument dependent were calculated materials diffractometer VULCAN (Spallation Neutron Source, Oak Ridge National Laboratory). QMC method applied face-centered cubic structures can be easily extended other crystallographic symmetries. Examples include 316LN stainless steelin situloaded in tension at room temperature an Al–2%Mg alloy, substantially deformed by cold rolling situannealed up 653 K.

参考文章(36)
G.B. Harris, X. Quantitative measurement of preferred orientation in rolled uranium bars Philosophical Magazine Series 1. ,vol. 43, pp. 113- 123 ,(1952) , 10.1080/14786440108520972
X.L. Wang, Thomas Holden, A.D. Stoica, K. An, H.D. Skorpenske, A.B. Jones, G.Q. Rennich, E.B. Iverson, First Results from the VULCAN Diffractometer at the SNS Materials Science Forum. ,vol. 652, pp. 105- 110 ,(2010) , 10.4028/WWW.SCIENTIFIC.NET/MSF.652.105
M.L Crow, J.P Hodges, R.G Cooper, Shifting scintillator prototype large pixel wavelength-shifting fiber detector for the POWGEN3 powder diffractometer Nuclear Instruments & Methods in Physics Research Section A-accelerators Spectrometers Detectors and Associated Equipment. ,vol. 529, pp. 287- 292 ,(2004) , 10.1016/J.NIMA.2004.04.167
G Winther, L Margulies, S Schmidt, H.F Poulsen, Lattice rotations of individual bulk grains Part II: correlation with initial orientation and model comparison Acta Materialia. ,vol. 52, pp. 2863- 2872 ,(2004) , 10.1016/J.ACTAMAT.2004.02.045
N. C. Popa, Texture in Rietveld refinement Journal of Applied Crystallography. ,vol. 25, pp. 611- 616 ,(1992) , 10.1107/S0021889892004795
X. Wang, F.J. Hickernell, Randomized Halton sequences Mathematical and Computer Modelling. ,vol. 32, pp. 887- 899 ,(2000) , 10.1016/S0895-7177(00)00178-3
A. Baczmanski, K. Wierzbanowski, J. Jura, W. G. Haije, R. B. Helmholdt, F. Maniawski, Calculation of the rotation rate field on the basis of experimental texture data Philosophical Magazine. ,vol. 67, pp. 155- 171 ,(1993) , 10.1080/01418619308207149
A. Clement, Prediction of deformation texture using a physical principle of conservatiol Materials Science and Engineering. ,vol. 55, pp. 203- 210 ,(1982) , 10.1016/0025-5416(82)90133-1