Hidden Superlattice in Tl2(SC6H4S) and Tl2(SeC6H4Se) Solved from Powder X-ray Diffraction

作者: Kevin H. Stone , Dayna L. Turner , Mayank Pratap Singh , Thomas P. Vaid , Peter W. Stephens

DOI: 10.1107/S0108768111030692

关键词: Square pyramidTriclinic crystal systemIsostructuralFormula unitX-ray crystallographyPowder diffractionChemistryCrystallographySuperlatticeCrystal structure

摘要: The crystal structures of the isostructural title compounds poly [(μ-benzene-1, 4-dithiolato) dithallium], Tl2 (SC6H4S), and poly [(μ-benzene-1, 4-diselenolato) dithallium], Tl2 …

参考文章(20)
Christoph Janiak, Roald Hoffmann, Thallium(I)-thallium(I) and indium(I)-indium(I) interactions: from the molecular to the solid state Journal of the American Chemical Society. ,vol. 112, pp. 5924- 5946 ,(1990) , 10.1021/JA00172A005
A. A. Coelho, Indexing of powder diffraction patterns by iterative use of singular value decomposition Journal of Applied Crystallography. ,vol. 36, pp. 86- 95 ,(2003) , 10.1107/S0021889802019878
Montana V. Childress, David Millar, Todd M. Alam, Kevin A. Kreisel, Glenn P. A. Yap, Lev N. Zakharov, James A. Golen, Arnold L. Rheingold, Linda H. Doerrer, Thallophilic interactions in aryloxide compounds: the [Tl2(mu2-OAr)4] structural motif in (TlOAr)4 and Tl2Cu(OAr)4 compounds. Inorganic Chemistry. ,vol. 45, pp. 3864- 3877 ,(2006) , 10.1021/IC050955O
Dieter Labahn, Ehmke Phol, Regine Herbst-Irmer, Dietmar Stalke, Herbert W. Roesky, George M. Sheldrick, Darstellung und Struktur von Thallium(I)‐2,4,6‐tris(trifluormethyl)thiophenolat, einer Verbindung mit faltblattartig‐polymerem Aufbau Chemische Berichte. ,vol. 124, pp. 1127- 1129 ,(1991) , 10.1002/CBER.19911240522
Boris E. Bosch, Martin Eisenhawer, Berthold Kersting, Kristin Kirschbaum, Bernt Krebs, Dean M. Giolando, Synthesis, Properties, and Crystal Structures of Benzene-1,2-dithiolato Complexes of Thallium(I) and -(III). Inorganic Chemistry. ,vol. 35, pp. 6599- 6605 ,(1996) , 10.1021/IC951411X
Adrienne Hammerschmidt, Andreas Brömmelhaus, Mechtild Läge, Bernt Krebs, Novel polynuclear thallium thiolates with cage structures Inorganica Chimica Acta. ,vol. 358, pp. 4247- 4252 ,(2005) , 10.1016/J.ICA.2005.03.038
Simon P. Westrip, publCIF: software for editing, validating and formatting crystallographic information files Journal of Applied Crystallography. ,vol. 43, pp. 920- 925 ,(2010) , 10.1107/S0021889810022120