作者: Ma Qiming
DOI:
关键词: Styrene 、 Alcohol 、 Organic chemistry 、 Chemistry 、 Hydrogenolysis 、 Salt (chemistry) 、 Propanediol 、 Ethylbenzene 、 Elimination reaction 、 Diethyl malonate
摘要: The invention provides a method to prepare compound method, including the steps: ethylbenzene and capryl chloride make Friedel-Crafts reaction generate p-capryl chloroethylbenzene; convert chloroethylbenzene under action of sodium iodide into iodoethylbenzene; iodoethylbenzene acetylamino diethyl malonate condense alkali 2-(p-capryl phenethyl)-2-acetylamino malonate; or makes elimination styrene, which together with condenses phenethyl)-2- is reduced 2-[4-(1-hydroxyoctyl) phenethyl-]2- propylene alcohol; other coumpound hydrogenolysis obtain 2-(p-octyl phenethyl)-acetylamino hydrolyzation then acidifies them salt, so as it. It also intermediate in above preparing course.