Detection of Zinc and Lead in Wine by Potentiometric Stripping on Novel Dental Amalgam Electrodes
作者： Øyvind Mikkelsen , Camilla Nordhei , Silje M. Skogvold , Knut H. Schrøder
DOI: 10.1081/AL-200035832
关键词: Wine 、 Amalgam (chemistry) 、 Zinc 、 Nuclear chemistry 、 Detection limit 、 Stripping (chemistry) 、 Analytical chemistry 、 Voltammetry 、 Atomic absorption spectroscopy 、 Chemistry 、 Potentiometric titration
摘要: Abstract A simple method for detection of zinc and lead in wine by use potentiometric stripping analyses (PSA) on the dental amalgam electrode is introduced demonstrated 10 different wines, both red white. The combination PSA novel nontoxic offers a fast easy‐to‐use technique without matrix effects seen in, e.g., voltammetry. Concentrations range approximately 2.1 × 10−6 M to 11.7 × 10−6 M (3.5% std. dev.) 9.7 × 10−8 M 2.4 × 10−7 M were found actual samples. measurements verified against atomic adsorption spectroscopy (AAS), good correlation factor was (r 2 = 0.96). speciation study performed measuring amount before after addition acid, giving an approximate ratio between free total metals. Estimated limits calculated to, respectively, 3.0 × 10−7 M 1.5 × 10−8 M ...
sci-hub.se 参考文章(33)
Salvatore Daniele, Maria-Antonietta Baldo, Paolo Ugo, Gian-Antonio Mazzocchin, Determination of heavy metals in real samples by anodic stripping voltammetry with mercury microelectrodes : Part 1. Application to Wine Analytica Chimica Acta. ,vol. 219, pp. 9- 18 ,(1989) , 10.1016/S0003-2670(00)80328-1
M. Ariel, U. Eisner, S. Gottesfeld, Trace analysis by anodic stripping voltammetry Journal of Electroanalytical Chemistry (1959). ,vol. 7, pp. 307- 314 ,(1964) , 10.1016/0022-0728(64)80105-4
Øyvind Mikkelsen, Knut H. Schrøder, Enhanced Mass Transport in Voltammetry by Use of Low Frequency Sound. The Relationship Between Sound Intensity and Current Response, Using External Sound Source Electroanalysis. ,vol. 12, pp. 1201- 1206 ,(2000) , 10.1002/1521-4109(200010)12:15<1201::AID-ELAN1201>3.0.CO;2-0
Ø. Mikkelsen, K. Schr⊘der, Dental Amalgam in Voltammetry. Some Preliminary Results Analytical Letters. ,vol. 33, pp. 3253- 3269 ,(2000) , 10.1080/00032719.2000.10399499
J. Jurasović, A. Pizent, Non-occupational lead poisoning in Croatia Toxicology Letters. ,vol. 78, pp. 44- 45 ,(1995) , 10.1016/0378-4274(95)94786-G
E Alonso Alvarez, M Callejón Mochón, JC Jiménez Sánchez, M Ternero Rodríguez, None, A Voltammetry Procedure with Medium Exchange for the Speciation of Heavy Metals in Wastewater of a Sewage Treatment Plant Electroanalysis. ,vol. 10, pp. 917- 920 ,(1998) , 10.1002/(SICI)1521-4109(199810)10:13<917::AID-ELAN917>3.0.CO;2-L
Myung-zoon Czae, Joseph Wang, Pushing the detectability of voltammetry: how low can we go? Talanta. ,vol. 50, pp. 921- 928 ,(1999) , 10.1016/S0039-9140(99)00205-2
Joseph Wang, Jianmin Lu, Baomin Tian, Chaim Yarnitzky, Screen-printed ultramicroelectrode arrays for on-site stripping measurements of trace metals Journal of Electroanalytical Chemistry. ,vol. 361, pp. 77- 83 ,(1993) , 10.1016/0022-0728(93)87040-3
Gian P.G Freschi, Carolina S Dakuzaku, Mercedes de Moraes, Joaquim A Nóbrega, José A Gomes Neto, Simultaneous determination of cadmium and lead in wine by electrothermal atomic absorption spectrometry Spectrochimica Acta Part B: Atomic Spectroscopy. ,vol. 56, pp. 1987- 1993 ,(2001) , 10.1016/S0584-8547(01)00331-7
Joanna Szpunar, Patrice Pellerin, Alexei Makarov, Thierry Doco, Pascale Williams, Bernard Medina, Ryszard Łobiński, Speciation analysis for biomolecular complexes of lead in wine by size-exclusion high-performance liquid chromatography-inductively coupled plasma mass spectrometry Journal of Analytical Atomic Spectrometry. ,vol. 13, pp. 749- 754 ,(1998) , 10.1039/A803038C