Characterization of composition and structure of clay minerals in sandstone with ptychographic X-ray nanotomography

作者: Wesley De Boever , Ana Diaz , Hannelore Derluyn , Tim De Kock , Jeroen Van Stappen

DOI: 10.1016/J.CLAY.2015.09.020

关键词: GroundwaterTomographyClay mineralsMicrostructureGeologySynchrotronWeatheringCharacterization (materials science)PorosityMineralogy

摘要: Abstract Three-dimensional analysis of microporous and fine-grained particles in natural stone is important for understanding their internal fluid flow processes to allow dynamics be modeled. These are great interest oil, gas groundwater studies, as well the weathering building materials. For features above 1 μm methods such X-ray micro-computed tomography (μ-CT) can provide non-destructive, quantitative analysis. Non-destructive 3D imaging at resolutions below 300–400 nm, however, has remained a challenge until recent developments synchrotron beam lines. In this paper we visualize microstructure clay mineral samples extracted from two different sandstones spatial down 45 nm, using ptychographic computed (PXCT). Furthermore, relative humidity environment during these experiments was controlled order assess its influence on analyzed samples. Based high-quality images, were able acquire non-destructively information content distribution, porosity connectivity clusters inside sandstone.

参考文章(49)
PÅL-ERIC ØREN, STIG BAKKE, Process based reconstruction of sandstones and prediction of transport properties Transport in Porous Media. ,vol. 46, pp. 311- 343 ,(2002) , 10.1023/A:1015031122338
Tero Harjupatana, Jarno Alaraudanjoki, Markku Kataja, X-ray tomographic method for measuring three-dimensional deformation and water content distribution in swelling clays Applied Clay Science. ,vol. 114, pp. 386- 394 ,(2015) , 10.1016/J.CLAY.2015.06.016
S. Zabihzadeh, S. Van Petegem, L.I. Duarte, R. Mokso, A. Cervellino, H. Van Swygenhoven, Deformation behavior of sintered nanocrystalline silver layers Acta Materialia. ,vol. 97, pp. 116- 123 ,(2015) , 10.1016/J.ACTAMAT.2015.06.040
Timothy Wangler, George W. Scherer, Clay swelling mechanism in clay-bearing sandstones Environmental Earth Sciences. ,vol. 56, pp. 529- 534 ,(2008) , 10.1007/S00254-008-1380-3
Xiaojing Huang, Hanfei Yan, Ross Harder, Yeukuang Hwu, Ian K. Robinson, Yong S. Chu, Optimization of overlap uniformness for ptychography Optics Express. ,vol. 22, pp. 12634- 12644 ,(2014) , 10.1364/OE.22.012634
Satoshi Tomioka, Tamotsu Kozaki, Hidenori Takamatsu, Natsuko Noda, Shusuke Nisiyama, Naofumi Kozai, Satoru Suzuki, Seichi Sato, Analysis of microstructural images of dry and water-saturated compacted bentonite samples observed with X-ray micro CT Applied Clay Science. ,vol. 47, pp. 65- 71 ,(2010) , 10.1016/J.CLAY.2008.09.001
Lukas M Keller, Philipp Schuetz, Rolf Erni, Marta D Rossell, Falk Lucas, Miriam Lucas, Philippe Gasser, Lorenz Holzer, Characterization of multi-scale microstructural features in Opalinus Clay Microporous and Mesoporous Materials. ,vol. 170, pp. 83- 94 ,(2013) , 10.1016/J.MICROMESO.2012.11.029
Manuel Guizar-Sicairos, Ian Johnson, Ana Diaz, Mirko Holler, Petri Karvinen, Hans-Christian Stadler, Roberto Dinapoli, Oliver Bunk, Andreas Menzel, High-throughput ptychography using Eiger: scanning X-ray nano-imaging of extended regions Optics Express. ,vol. 22, pp. 14859- 14870 ,(2014) , 10.1364/OE.22.014859
J. M. Rodenburg, H. M. L. Faulkner, A phase retrieval algorithm for shifting illumination Applied Physics Letters. ,vol. 85, pp. 4795- 4797 ,(2004) , 10.1063/1.1823034