Polishing of Ground Y-TZP Ceramic is Mandatory for Improving the Mechanical Behavior.

作者: Camila Pauleski Zucuni , Luis Felipe Guilardi , Marilia Pivetta Rippe , Gabriel Kalil Rocha Pereira , Luiz Felipe Valandro

DOI: 10.1590/0103-6440201802044

关键词: CeramicFlexural strengthSurface finishDiamondGlazingPolishingMaterials scienceComposite materialGrindingWeibull modulus

摘要: It evaluated the effect of aging by Low Temperature Degradation (LTD), executed after post- processing surface treatments (polishing, heat treatment and glazing), on characteristics (micromorphology roughness) structural stability (phase transformation mechanical behavior-flexural strength reliability) a ground yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) ceramic. Discs Y-TZP (VITA In-Ceram YZ) were manufactured (ISO:6872-2015; 15 mm in diameter 1.2 ± 0.2 thickness) randomly assigned into 10 groups according two factors: "aging" 2 levels (with or without) "surface treatment" 5 (Ctrl: as-sintered; Gr: grinding with coarse diamond bur; Gr + HT: plus treatment; Pol: polishing; Gl: glazing). Roughness (n=30), biaxial flexural test phase (n=2), topography (n=2) analyses performed. Aging led to an intense increase monoclinic (m) content for all tested conditions, being as-sintered samples (Ctrl= 65.6%) more susceptible t-m transformation. Despite increasing m-phase content, was not detrimental characteristic (except condition). There no significant reduction Weibull modulus treatments. Additionally, glazing decrease strength, while polishing presented highest values. Thus, is mandatory ceramic, performing heat-treatment alone lead worst performance.

参考文章(21)
J.A. Muñoz-Tabares, M. Anglada, Hydrothermal degradation of ground 3Y-TZP Journal of The European Ceramic Society. ,vol. 32, pp. 325- 333 ,(2012) , 10.1016/J.JEURCERAMSOC.2011.08.029
Noxy George Manjuran, T. Sreelal, An In Vitro Study to Identify a Ceramic Polishing Protocol Effecting Smoothness Superior to Glazed Surface The Journal of Indian Prosthodontic Society. ,vol. 14, pp. 219- 227 ,(2014) , 10.1007/S13191-013-0313-3
Massimiliano Guazzato, Linda Quach, Mohammad Albakry, Michael V. Swain, Influence of surface and heat treatments on the flexural strength of Y-TZP dental ceramic Journal of Dentistry. ,vol. 33, pp. 9- 18 ,(2005) , 10.1016/J.JDENT.2004.07.001
GKR Pereira, M Amaral, PF Cesar, MC Bottino, CJ Kleverlaan, LF Valandro, Effect of low-temperature aging on the mechanical behavior of ground Y-TZP Journal of The Mechanical Behavior of Biomedical Materials. ,vol. 45, pp. 183- 192 ,(2015) , 10.1016/J.JMBBM.2014.12.009
Thomaz Kosmac, Rudolf Wagner, Nils Claussen, X‐Ray Determination of Transformation Depths in Ceramics Containing Tetragonal ZrO2 Journal of the American Ceramic Society. ,vol. 64, ,(1981) , 10.1111/J.1151-2916.1981.TB10285.X
K KOBAYASHI, H KUWAJIMA, T MASAKI, Phase change and mechanical properties of ZrO2-Y2O3 solid electrolyte after ageing Solid State Ionics. pp. 489- 493 ,(1981) , 10.1016/0167-2738(81)90138-7
JA Muñoz-Tabares, E Jiménez-Piqué, J Reyes-Gasga, M Anglada, Microstructural changes in ground 3Y-TZP and their effect on mechanical properties Acta Materialia. ,vol. 59, pp. 6670- 6683 ,(2011) , 10.1016/J.ACTAMAT.2011.07.024
Hideo Toraya, Masahiro Yoshimura, Shigeyuki Somiya, Calibration Curve for Quantitative Analysis of the Monoclinic‐Tetragonal ZrO2 System by X‐Ray Diffraction Journal of the American Ceramic Society. ,vol. 67, ,(1984) , 10.1111/J.1151-2916.1984.TB19715.X
RONALD C. GARVIE, PATRICK S. NICHOLSON, Phase Analysis in Zirconia Systems Journal of the American Ceramic Society. ,vol. 55, pp. 303- 305 ,(1972) , 10.1111/J.1151-2916.1972.TB11290.X
C. Piconi, G. Maccauro, Zirconia as a ceramic biomaterial Biomaterials. ,vol. 20, pp. 1- 25 ,(1999) , 10.1016/S0142-9612(98)00010-6