Low temperature consolidation of hydroxyapatite-reduced graphene oxide nano-structured powders
作者： Hassan Nosrati , Rasoul Sarraf-Mamoory , Reza Zolfaghari Emameh , Dang Quang Svend Le , Maria Canillas Perez
DOI: 10.1039/D0MA00212G
关键词:
摘要: In this study, hydroxyapatite-reduced graphene oxide (HA-rGO) powders were first synthesized in situ using a hydrothermal method. These then consolidated cold sintering The solvent used method was water + dimethylformamide brushite which added to the at different ratios. sintered samples evaluated X-ray diffraction, Fourier transform infrared spectroscopy, Raman high-resolution transmission electron microscopy, and Vickers microindentation. results of study showed that best conditions for rGO-HA nanopowders temperature 200 °C, holding time >30 min, pressure 500 MPa. mechanical properties achieved when content considered be 20 wt%. Crack deflection bridging among mechanisms increased fracture toughness these nanocomposites. By adding 1.5% rGO, nanocomposite (using method) approximately equivalent spark plasma HA.
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sci-hub.st 参考文章(73)
M SHIRKHANZADEH, Direct formation of nanophase hydroxyapatite on cathodically polarized electrodes. Journal of Materials Science: Materials in Medicine. ,vol. 9, pp. 67- 72 ,(1998) , 10.1023/A:1008838813120
M Jevtic, M Mitric, S Skapin, B Jancar, N Ignjatovic, D Uskokovic, None, Crystal Structure of Hydroxyapatite Nanorods Synthesized by Sonochemical Homogeneous Precipitation Crystal Growth & Design. ,vol. 8, pp. 2217- 2222 ,(2008) , 10.1021/CG7007304
T.Anee Kuriakose, S.Narayana Kalkura, M. Palanichamy, D. Arivuoli, Karsten Dierks, G. Bocelli, C. Betzel, Synthesis of stoichiometric nano crystalline hydroxyapatite by ethanol-based sol–gel technique at low temperature Journal of Crystal Growth. ,vol. 263, pp. 517- 523 ,(2004) , 10.1016/J.JCRYSGRO.2003.11.057
Xiaojun Guo, Hudong Yan, Shengguo Zhao, Zhang Li, Yutian Li, Xiaohu Liang, Effect of calcining temperature on particle size of hydroxyapatite synthesized by solid-state reaction at room temperature Advanced Powder Technology. ,vol. 24, pp. 1034- 1038 ,(2013) , 10.1016/J.APT.2013.03.002
Isao Kimura, Synthesis of Hydroxyapatite by Interfacial Reaction in a Multiple Emulsion Research Letters in Materials Science. ,vol. 2007, pp. 1- 4 ,(2007) , 10.1155/2007/71284
A. JILLAVENKATESA, A. JILLAVENKATESA, Sol–gel processing of hydroxyapatite Journal of Materials Science. ,vol. 33, pp. 4111- 4119 ,(1998) , 10.1023/A:1004436732282
Yuan-Liang Chin, Wei-Hsing Tuan, Feasibility of Using Multilayer Platelets as Toughening Agents Materials. ,vol. 3, pp. 1- 8 ,(2009) , 10.3390/MA3010001
Kimihiro Yamashita, Tomohiro Arashi, Kazuhisa Kitagaki, Shinji Yamada, Takao Umegaki, Kenji Ogawa, Preparation of Apatite Thin Films through rf-Sputtering from Calcium Phosphate Glasses Journal of the American Ceramic Society. ,vol. 77, pp. 2401- 2407 ,(1994) , 10.1111/J.1151-2916.1994.TB04611.X
A.J. Ruys, M. Wei, C.C. Sorrell, M.R. Dickson, A. Brandwood, B.K. Milthorpe, Sintering effects on the strength of hydroxyapatite Biomaterials. ,vol. 16, pp. 409- 415 ,(1995) , 10.1016/0142-9612(95)98859-C
Daniel O. Costa, S. Jeffrey Dixon, Amin S. Rizkalla, One- and three-dimensional growth of hydroxyapatite nanowires during sol-gel-hydrothermal synthesis. ACS Applied Materials & Interfaces. ,vol. 4, pp. 1490- 1499 ,(2012) , 10.1021/AM201735K