Preparation of monodisperse peanut-type α-Fe2O3 particles from condensed ferric hydroxide gel

作者: Tadao Sugimoto , Mohammad M. Khan , Atsushi Muramatsu

DOI: 10.1016/0927-7757(93)80285-M

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摘要: Recently, it has been found that monodisperse pseudocubic hematite particles 1.65 μm in mean edge length can be obtained large quantities of the order molality with a yield close to 100%, by adding 100 ml 5.4 N NaOH well-stirred 2.0 M FeCl3 and aging resulting condensed gel Fe(OH)3 for 8 days at 100°C. The method was provisionally referred as gel—sol method. As an application this technique, when 90 6.0 10 sulfate or phosphate solution were added instead NaOH, turned into peanut-type via ellipsoidal shape increasing concentration additives.

参考文章(2)
Tadao Sugimoto, Kazuo Sakata, Preparation of monodisperse pseudocubic α-Fe2O3 particles from condensed ferric hydroxide gel Journal of Colloid and Interface Science. ,vol. 152, pp. 587- 590 ,(1992) , 10.1016/0021-9797(92)90062-Q
Masataka Ozaki, Stanka Kratohvil, Egon Matijević, Formation of monodispersed spindle-type hematite particles joint international conference on information sciences. ,vol. 102, pp. 146- 151 ,(1984) , 10.1016/0021-9797(84)90208-X