Fully Integrated Flexible Dielectric Monitoring Sensor System for Real-Time In Situ Prediction of the Degree of Cure and Glass Transition Temperature of an Epoxy Resin

作者: Lode Daelemans , Diana-Elena Mogosanu , Bart Plovie , Karen De Clerck , Thomas Vervust

DOI: 10.1109/TIM.2021.3057291

关键词:

摘要: Flexible dielectric sensors received significant interest for real-time in situ cure monitoring of polymeric composites over the past decade. Currently, state-of-the-art mainly focus on detecting distinct stages composite curing process. While low-cost and quantitative thermal, mechanical, chemical properties materials during is great interest, to date, such a sensor system has not been realized because existing devices excessively depend external instrumentations, combined with lack an embedded reliable data processing module. Here, fully integrated (DMS) incorporating temperature developed, capable temperature, degree cure, glass transition ( $T_{g}$ ) composites. An independent characterization kinetics was performed using differential scanning calorimetry Raman spectroscopy. These enabled associating main physical transformations particular features observed measurements. We demonstrate accurate estimation epoxy resin. The proposed shows potential new generation intelligent manufacturing technology materials.

参考文章(31)
George M. Maistros, Ivana K. Partridge, Monitoring autoclave cure in commercial carbon fibre/epoxy composites Composites Part B: Engineering. ,vol. 29, pp. 245- 250 ,(1998) , 10.1016/S1359-8368(97)00020-6
Jérôme Fournier, Graham Williams, Christine Duch, George Anthony Aldridge, Changes in molecular dynamics during bulk polymerization of an epoxide-amine system as studied by dielectric relaxation spectroscopy Macromolecules. ,vol. 29, pp. 7097- 7107 ,(1996) , 10.1021/MA9517862
Y. Yang, G. Chiesura, G. Luyckx, T. Vervust, F. Bossuyt, M. Kaufmann, J. Degrieck, J. Vanfleteren, Development of a Dielectric Sensor System for the On-line Cure Monitoring of Composites Procedia Technology. ,vol. 15, pp. 631- 637 ,(2014) , 10.1016/J.PROTCY.2014.09.024
David R. Day, Dielectric determination of cure state during non-isothermal cure Polymer Engineering and Science. ,vol. 29, pp. 334- 338 ,(1989) , 10.1002/PEN.760290512
A McIlhagger, D Brown, B Hill, The development of a dielectric system for the on-line cure monitoring of the resin transfer moulding process Composites Part A-applied Science and Manufacturing. ,vol. 31, pp. 1373- 1381 ,(2000) , 10.1016/S1359-835X(00)00050-6
Goker Tuncol, Murat Danisman, Alper Kaynar, E. Murat Sozer, Constraints on monitoring resin flow in the resin transfer molding (RTM) process by using thermocouple sensors Composites Part A-applied Science and Manufacturing. ,vol. 38, pp. 1363- 1386 ,(2007) , 10.1016/J.COMPOSITESA.2006.10.009
Bekir Yenilmez, E. Murat Sozer, A grid of dielectric sensors to monitor mold filling and resin cure in resin transfer molding Composites Part A-applied Science and Manufacturing. ,vol. 40, pp. 476- 489 ,(2009) , 10.1016/J.COMPOSITESA.2009.01.014
Seiji Kobayashi, Ryosuke Matsuzaki, Akira Todoroki, Multipoint cure monitoring of CFRP laminates using a flexible matrix sensor Composites Science and Technology. ,vol. 69, pp. 378- 384 ,(2009) , 10.1016/J.COMPSCITECH.2008.10.029
M. B. M. Mangion, G. P. Johari, Relaxations of thermosets. IV. A dielectric study of crosslinking of diglycidyl ether of bisphenol-a by two curing agents Journal of Polymer Science Part B: Polymer Physics. ,vol. 28, pp. 1621- 1639 ,(1990) , 10.1002/POLB.1990.090280916