Hollow-fiber liquid-phase microextraction combined with capillary electrophoresis for trace analysis of sulfonamide compounds
作者： Fanghong Tong , Yang Zhang , Fang Chen , Ying Li , Guanhua Ma
DOI: 10.1016/J.JCHROMB.2013.10.038
关键词:
摘要: A hollow-fiber liquid-phase microextraction (HF-LPME) method has been developed for the preconcentration of trace sulfonamides in water samples. Six commonly used including sulfamethazine (SMZ), sulfamerazine (SMR), sulfadiazine (SDZ), sulfadimethoxine (SDM), sulfamethoxazole (SMX), and sulfathiazole (STZ) were determined by CE with electrochemical detection (CE-ED) after microextraction. Several factors that affect extraction efficiency, separation, investigated. Under optimum conditions, above sulfonamide compounds could achieve baseline separation within 35min, exhibiting a linear calibration over three orders magnitude (r(2)≥0.998); obtained enrichment between 121 (for SDZ) 996 SDM), LODs range 0.033-0.44ng/mL. The proposed HF-LPME/CE-ED applied sensitive analyses real-world samples recoveries 75.1-109%.
elsevier.com
sci-hub.se 参考文章(30)
Jingyi Lee, Hian Kee Lee, Knut E. Rasmussen, Stig Pedersen-Bjergaard, Environmental and bioanalytical applications of hollow fiber membrane liquid-phase microextraction: a review. Analytica Chimica Acta. ,vol. 624, pp. 253- 268 ,(2008) , 10.1016/J.ACA.2008.06.050
Antonio V. Herrera-Herrera, Javier Hernández-Borges, Teresa M. Borges-Miquel, Miguel Ángel Rodríguez-Delgado, Dispersive liquid–liquid microextraction combined with ultra-high performance liquid chromatography for the simultaneous determination of 25 sulfonamide and quinolone antibiotics in water samples Journal of Pharmaceutical and Biomedical Analysis. ,vol. 75, pp. 130- 137 ,(2013) , 10.1016/J.JPBA.2012.11.026
Yong Tao, Jing-Fu Liu, Xia-Lin Hu, Hong-Cheng Li, Thanh Wang, Gui-Bin Jiang, Hollow fiber supported ionic liquid membrane microextraction for determination of sulfonamides in environmental water samples by high-performance liquid chromatography Journal of Chromatography A. ,vol. 1216, pp. 6259- 6266 ,(2009) , 10.1016/J.CHROMA.2009.06.025
Mª Jesús García-Galán, M. Silvia Díaz-Cruz, Damià Barceló, Damià Barceló, Combining chemical analysis and ecotoxicity to determine environmental exposure and to assess risk from sulfonamides Trends in Analytical Chemistry. ,vol. 28, pp. 804- 819 ,(2009) , 10.1016/J.TRAC.2009.04.006
María Ramos Payán, Miguel Ángel Bello López, Rut Fernández-Torres, Mercedes Villar Navarro, Manuel Callejón Mochón, Hollow fiber-based liquid phase microextraction (HF-LPME) for a highly sensitive HPLC determination of sulfonamides and their main metabolites Journal of Chromatography B. ,vol. 879, pp. 197- 204 ,(2011) , 10.1016/J.JCHROMB.2010.12.006
Naziha Assassi, Amel Tazerouti, Jean Paul Canselier, Analysis of chlorinated, sulfochlorinated and sulfonamide derivatives of n-tetradecane by gas chromatography/mass spectrometry Journal of Chromatography A. ,vol. 1071, pp. 71- 80 ,(2005) , 10.1016/J.CHROMA.2005.01.102
A.A.M. Stolker, U.A.Th. Brinkman, Analytical strategies for residue analysis of veterinary drugs and growth-promoting agents in food-producing animals - A review Journal of Chromatography A. ,vol. 1067, pp. 15- 53 ,(2005) , 10.1016/J.CHROMA.2005.02.037
J. Raich-Montiu, J. Folch, R. Compañó, M. Granados, M.D. Prat, Analysis of trace levels of sulfonamides in surface water and soil samples by liquid chromatography-fluorescence Journal of Chromatography A. ,vol. 1172, pp. 186- 193 ,(2007) , 10.1016/J.CHROMA.2007.10.010
Qingcui Chu, Dongli Zhang, Jinyan Wang, Jiannong Ye, Multi-residue analysis of sulfonamides in animal tissues by capillary zone electrophoresis with electrochemical detection Journal of the Science of Food and Agriculture. ,vol. 89, pp. 2498- 2504 ,(2009) , 10.1002/JSFA.3756
Soparat Yudthavorasit, Chayada Chiaochan, Natchanun Leepipatpiboon, Simultaneous determination of multi-class antibiotic residues in water using carrier-mediated hollow-fiber liquid-phase microextraction coupled with ultra-high performance liquid chromatography tandem mass spectrometry Mikrochimica Acta. ,vol. 172, pp. 39- 49 ,(2011) , 10.1007/S00604-010-0454-6