4-Hexyl-oxybenzamide.

作者: Huey Chong Kwong , Mohamad Zaki Ab. Rahman , Mohamed Ibrahim Mohamed Tahir , Sidik Silong

DOI: 10.1107/S1600536811003096

关键词:

摘要: In the title compound, C13H19NO2, dihedral angle between benzene ring and plane throught non-H atoms of amide group is 29.3 (1)°. The alkane carbon skeleton are twisted slightly with respect to each other [5.40 (5)°]. crystal, mol­ecules oriented groups head-to-head, forming N—H⋯O hydrogen-bonded dimers. dimers connected by further hydrogen bonds into a ladder-like motif along b axis.

参考文章(10)
Klaus Merz, 1-Phenyl­decane Acta Crystallographica Section E-structure Reports Online. ,vol. 58, ,(2002) , 10.1107/S1600536802004725
Catherine Pala Wilgus, Susan Downing, Erich Molitor, Satinder Bains, Richard M. Pagni, George W. Kabalka, The acid-catalyzed and uncatalyzed hydrolysis of nitriles on unactivated alumina Tetrahedron Letters. ,vol. 36, pp. 3469- 3472 ,(1995) , 10.1016/0040-4039(95)00528-K
A. Altomare, G. Cascarano, C. Giacovazzo, A. Guagliardi, M. C. Burla, G. Polidori, M. Camalli, SIR92 – a program for automatic solution of crystal structures by direct methods Journal of Applied Crystallography. ,vol. 27, pp. 435- 435 ,(1994) , 10.1107/S002188989400021X
Silvina Pagola, Peter W. Stephens, Herringbone array of hydrogen-bonded ribbons in 2-ethoxybenzamide from high-resolution X-ray powder diffraction. Acta Crystallographica Section C-crystal Structure Communications. ,vol. 65, ,(2009) , 10.1107/S0108270109040803
H. Gallardo, I. M. Begnini, The Synthesis and Liquid Crystal Properties of Some Series Homologues of 1,2,4-Oxadiazole Derivatives Molecular Crystals and Liquid Crystals. ,vol. 258, pp. 85- 94 ,(1995) , 10.1080/10587259508034550
Clare F. Macrae, Paul R. Edgington, Patrick McCabe, Elna Pidcock, Greg P. Shields, Robin Taylor, Matthew Towler, Jacco van de Streek, Mercury: visualization and analysis of crystal structures Journal of Applied Crystallography. ,vol. 39, pp. 453- 457 ,(2006) , 10.1107/S002188980600731X
Paul W. Betteridge, J. Robert Carruthers, Richard I. Cooper, Keith Prout, David J. Watkin, CRYSTALS version 12: software for guided crystal structure analysis Journal of Applied Crystallography. ,vol. 36, pp. 1487- 1487 ,(2003) , 10.1107/S0021889803021800
Peter G. Jones, Holger Thönnessen, Reinhard Schmutzler, Axel K. Fischer, A second polymorph of p-nitro­benz­amide Acta Crystallographica Section E-structure Reports Online. ,vol. 58, ,(2002) , 10.1107/S1600536802021244
Frank H. Allen, Olga Kennard, David G. Watson, Lee Brammer, A. Guy Orpen, Robin Taylor, Tables of bond lengths determined by X-ray and neutron diffraction. Part 1. Bond lengths in organic compounds Journal of The Chemical Society-perkin Transactions 1. ,(1987) , 10.1039/P298700000S1