Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid

作者: Marcel Sonneck , Tim Peppel , Anke Spannenberg , Sebastian Wohlrab

DOI: 10.3390/CRYST5040466

关键词:

摘要: The molecular structures of (E)-non-2-enoic acid (C9) and (E)-dec-2-enoic (C10) are reported. title compounds were crystallized by slow evaporation ethanolic solutions at −30 °C. C9 crystallizes in the monoclinic space group P21/c C10 triclinic P-1, each with 4 molecules unit cell. cell parameters for are: a = 10.6473(4) A, b 5.2855(2) c 17.0313(7) A; β 106.0985(10)° V 920.87(6) A3. 4.1405(2) 15.2839(6) 17.7089(7) α 68.3291(11)°, 83.3850(13)°, γ 85.0779(12)° 1033.39(8)

参考文章(33)
George O. Burr, Mildred M. Burr, Elmer S. Miller, ON THE FATTY ACIDS ESSENTIAL IN NUTRITION. III Journal of Biological Chemistry. ,vol. 97, pp. 1- 9 ,(1932) , 10.1016/S0021-9258(18)76213-3
Marcel Sonneck, Tim Peppel, Anke Spannenberg, Sebastian Wohlrab, Crystal structure of (E)-dodec-2-enoic acid Acta Crystallographica Section E: Crystallographic Communications. ,vol. 71, ,(2015) , 10.1107/S2056989015011937
Tonya C. Murphy, Claire Poppe, James E. Porter, Thomas J. Montine, Matthew J. Picklo Sr, 4‐Hydroxy‐trans‐2‐nonenoic acid is a γ‐hydroxybutyrate receptor ligand in the cerebral cortex and hippocampus Journal of Neurochemistry. ,vol. 89, pp. 1462- 1470 ,(2004) , 10.1111/J.1471-4159.2004.02442.X
Susan Tolnai, Gordon F. Townsend, Joseph F. Morgan, Helen J. Morton, Barbara Hazlett, R. W. Shuel, Studies on the in vitro Antitumor Activity of Fatty Acids: I. 10-Hydroxy-2-decenoic Acid from Royal Jelly Cancer Research. ,vol. 20, pp. 503- 510 ,(1960)
Andrew D. Bond, On the crystal structures and melting point alternation of the n-alkyl carboxylic acids New Journal of Chemistry. ,vol. 28, pp. 104- 114 ,(2004) , 10.1039/B307208H
Iain D. H. Oswald, Andrew J. Urquhart, Polymorphism and polymerisation of acrylic and methacrylic acid at high pressure CrystEngComm. ,vol. 13, pp. 4503- 4507 ,(2011) , 10.1039/C1CE05295K
Christer B. Aakeröy, Alicia M. Beatty, Brian A. Helfrich, Mark Nieuwenhuyzen, Do polymorphic compounds make good cocrystallizing agents? A structural case study that demonstrates the importance of synthon flexibility Crystal Growth & Design. ,vol. 3, pp. 159- 165 ,(2003) , 10.1021/CG025593Z
Arthur A. Spector, Hee-Yong Kim, Discovery of essential fatty acids Journal of Lipid Research. ,vol. 56, pp. 11- 21 ,(2015) , 10.1194/JLR.R055095
Yōzō Chatani, Yoshiaki Sakata, Isamu Nitta, Crystal structures of monomers polymerizable in their solid states. Part I. Acrylic acid Journal of Polymer Science Part B: Polymer Letters. ,vol. 1, pp. 419- 421 ,(1963) , 10.1002/POL.1963.110010805
M. A. Higgs, R. L. Sass, The crystal structure of acrylic acid Acta Crystallographica. ,vol. 16, pp. 657- 661 ,(1963) , 10.1107/S0365110X63001717