The AgcorePdshell bimetallic nanoparticles: simple biological synthesis and characterization

作者: Khalil Farhadi , Reza Emamali Sabzi , Mehrdad Forough , Atefeh Pourhossein , Rahim Molaei

DOI: 10.1007/S13738-015-0676-Y

关键词:

摘要: In this work and for the first time, bimetallic Ag–Pd nanoparticles equipped with a core–shell structure were prepared biologically by employing galvanic displacement reaction in which added PdCl2 reacts an Ag nanotemplate containing adsorbed soaproot (Acanthe phylum bracteatum) extract. Four samples different Ag/Pd molar ratios of 100:2, 100:5, 100:10 100:15 to synthesize structure. The characterized using UV–visible spectroscopy (UV–Vis), X-ray diffraction (XRD), scanning electron microscopy energy-dispersive (SEM–EDX), transmission (TEM) Fourier transform infrared (FTIR) analysis. results from UV–Vis revealed optimal ratio Ag/Pd, is appropriate prepare FTIR XRD confirmed pure formation. images TEM depicted spherical uniformly shaped without any agglomeration particle size 15 nm.

参考文章(54)
Robert L. Snyder, Ron Jenkins, Introduction to X-ray powder diffractometry ,(1996)
Kenneth J Klabunde, Ryan M Richards, Nanoscale materials in chemistry Nanoscale Materials in Chemistry. pp. 304- ,(2001) , 10.1002/0471220620
D Burckhardt, P Lauterer, The jumping plant-lice of Iran (Homoptera, Psylloidea). Revue Suisse De Zoologie. ,vol. 100, pp. 829- 898 ,(1993) , 10.5962/BHL.PART.79887
Paul Mulvaney, Surface Plasmon Spectroscopy of Nanosized Metal Particles Langmuir. ,vol. 12, pp. 788- 800 ,(1996) , 10.1021/LA9502711
Masoud Salavati-Niasari, Jaber Javidi, Synthesis of Hollow SiO2 Nanoparticles from Dy2O3@SiO2 Core–Shell Nanocomposites via a Recyclable Sonochemical Method Journal of Cluster Science. ,vol. 23, pp. 1019- 1028 ,(2012) , 10.1007/S10876-012-0490-Y
Yaokun Xiao, Baicheng Weng, Gang Yu, Jinyin Wang, Bonian Hu, Zongzhang Chen, Electrodeposition of Pd–Ag alloy nanowires on highly oriented pyrolytic graphite Journal of Applied Electrochemistry. ,vol. 36, pp. 807- 812 ,(2006) , 10.1007/S10800-006-9137-8
Omid Amiri, Masoud Salavati-Niasari, S. Mostafa Hosseinpour-Mashkani, Ali Rafiei, Samira Bagheri, Cadmium selenide@sulfide nanoparticle composites: Facile precipitation preparation, characterization, and investigation of their photocatalyst activity Materials Science in Semiconductor Processing. ,vol. 27, pp. 261- 266 ,(2014) , 10.1016/J.MSSP.2014.06.020
Sang Woo Han, Yunsoo Kim, Kwan Kim, Dodecanethiol-Derivatized Au/Ag Bimetallic Nanoparticles: TEM, UV/VIS, XPS, and FTIR Analysis. joint international conference on information sciences. ,vol. 208, pp. 272- 278 ,(1998) , 10.1006/JCIS.1998.5812
Orla M. Wilson, Robert W. J. Scott, Joaquin C. Garcia-Martinez, Richard M. Crooks, Synthesis, Characterization, and Structure-Selective Extraction of 1--3-nm Diameter AuAg Dendrimer-Encapsulated Bimetallic Nanoparticles Journal of the American Chemical Society. ,vol. 127, pp. 1015- 1024 ,(2005) , 10.1021/JA045224M