The high yield synthesis of an unsaturated osmium cluster; the X-ray crystal structure of [Os3(CO)8(H){Ph2PCH2P(Ph)C6H4}]
作者： Jennifer A. Clucas , Douglas F. Foster , Marjorie M. Harding , Anthony K. Smith
DOI: 10.1039/C39840000949
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摘要: Thermolysis of [Os3(CO)10(dppm)](dppm = Ph2PCH2PPh2) in refluxing toluene affords a high yield the unsaturated cluster [Os3(CO)8(H){Ph2PCH2P(Ph)C6H4}] which has been characterized by X-ray crystallography, and undergoes facile reversible reaction with CO.
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