Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane
作者： Fei Ye , Chang-Ying Sun , Ying Fu
DOI: 10.1155/2013/974174
关键词:
摘要: A new compound, 2-dichloromethyl-2-p-nitrophenyl-1,3-dioxane, was synthesized and characterized. The crystal structure of the title compound (C11H11Cl2NO4, ) has been determined by single-crystal X-ray diffraction. is monoclinic, space group with Å, °, , , mg/cm3, final for observed reflections . total 12162 were collected, which 2867 unique ().
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I. Jablonkai, K.K. Hatzios, Microsomal Oxidation of the Herbicides EPTC and Acetochlor and of the Safener MG-191 in Maize Pesticide Biochemistry and Physiology. ,vol. 48, pp. 98- 109 ,(1994) , 10.1006/PEST.1994.1011
Z Ekler, F Dutka, GR Stephenson, None, Safener effects on acetochlor toxicity, uptake, metabolism and glutathione S-transferase activity in maize Weed Research. ,vol. 33, pp. 311- 318 ,(1993) , 10.1111/J.1365-3180.1993.TB01946.X
Fei Ye, Ying Li, Ying Fu, Shuang Gao, Li-Xia Zhao, Microwave-Assisted Synthesis and Crystal Structure of Novel 2-Dichloromethyl-1,3-dioxolanes. ChemInform. ,vol. 44, ,(2013) , 10.1002/CHIN.201320136
István Jablonkai, Ferenc Dutka, Uptake, translocation, and metabolism of MG-191 safener in corn (Zea mays L.) Weed Science. ,vol. 43, pp. 169- 174 ,(1995) , 10.1017/S0043174500081017
Ying Fu, Fei Ye, Ying Li, Shuang Gao, Li-Xia Zhao, MICROWAVE-ASSISTED SYNTHESIS AND CRYSTAL STRUCTURE OF NOVEL 2-DICHLOROMETHYL-1,3-DIOXOLANES Heterocycles. ,vol. 87, pp. 407- 415 ,(2013) , 10.3987/COM-12-12628
Majid Moghadam, Iraj Mohammadpoor-Baltork, Shahram Tangestaninejad, Valiollah Mirkhani, Parvin Yazdani, Saeedeh Ghorjipoor, Highly efficient and chemoselective acetalization of carbonyl compounds catalyzed by new and reusable zirconyl triflate, ZrO(OTf)2 Heteroatom Chemistry. ,vol. 20, pp. 131- 135 ,(2009) , 10.1002/HC.20523
Silica Gel-Supported Metallic Sulfates Catalyzed Chemoselective Acetalization of Aldehydes under Microwave Irradiation Synlett. ,vol. 2000, pp. 0701- 0703 ,(2000) , 10.1055/S-2000-6617
Massimo Curini, Francesco Epifano, Maria Carla Marcotullio, Ornelio Rosati, An Efficient Procedure for the Preparation of Cyclic Ketals and Thioketals Catalyzed by Zirconium Sulfophenyl Phosphonate Synlett. ,vol. 2001, pp. 1182- 1184 ,(2001) , 10.1055/S-2001-15155
Bertrand Pério, Marie-Joelle Dozias, Patrick jacquault, Jack Hamelin, Solvent free protection of carbonyl group under microwave irradiation Tetrahedron Letters. ,vol. 38, pp. 7867- 7870 ,(1997) , 10.1016/S0040-4039(97)10149-6