INDIRECT ELECTROCHEMICAL OXIDATION OF 4-PICOLINE AND ITS N-OXIDE TO PYRIDINE-4-ALDEHYDE DIACETATE WITH ELECTROGENERATED COBALT(III) ACETATE IN AN IN-C ELL PROCESS
作者： Eberhard Steckhan , Magdi Abdel Azzem
DOI: 10.3987/COM-90-5489
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摘要: The indirect electrooxidation of 4-picoline and its N-oxide with in situ electrogenerated Co(III) acetate has been studied. Pyridine-4-aldehyde diacetate was obtained good yield (45-68%), if the electrolysis performed acetic anhydride at 80°C an undivided cell under controlled current conditions
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