3,3′-(Diazene-1,2-diyl)bis[4-(nitroamino)-1,2,5-oxadiazole 2-oxide]
作者： Alexander Larin , Igor Ovchinnikov , Leonid Fershtat , Nina Makhova
DOI: 10.3390/M1003
关键词:
摘要: The nitramino derivatives of furoxans are specific interest as precursors for the preparation high energy salts with nitrogen-rich cations. In this communication, 3,3′-(diazene-1,2-diyl)bis[4-(nitroamino)-1,2,5-oxadiazole 2-oxide] was prepared via nitration available 4,4′-diamino-3,3′-diazenofuroxan; best yield target compound achieved under action nitrating system HNO3/(CF3CO)2O in molar ratio 15:3 CCl4 at −5 °C. structure confirmed by means 1H, 13C,14N-NMR, IR spectroscopy and resolution mass spectra (HRMS).
mdpi.com
sci-hub.se 参考文章(14)
D. V. Dashko, A. I. Stepanov, A. A. Astrat'ev, 3,4-Bis(4'-nitrofurazan-3'-yl)furoxan: a Melt Cast Powerful Explosive and a Valuable Building Block in 1,2,5-Oxadiazole Chemistry Central European Journal of Energetic Materials. ,vol. 9, pp. 329- 342 ,(2012)
Dennis Fischer, Thomas M. Klapötke, Jörg Stierstorfer, Synthesis and Characterization of Diaminobisfuroxane European Journal of Inorganic Chemistry. ,vol. 2014, pp. 5808- 5811 ,(2014) , 10.1002/EJIC.201402960
Lixuan Liang, Kai Wang, Chengming Bian, Liming Ling, Zhiming Zhou, 4‐Nitro‐3‐(5‐tetrazole)furoxan and Its Salts: Synthesis, Characterization, and Energetic Properties Chemistry: A European Journal. ,vol. 19, pp. 14902- 14910 ,(2013) , 10.1002/CHEM.201301042
Bo Wu, Hongwei Yang, Qiuhan Lin, Zhixin Wang, Chunxu Lu, Guangbin Cheng, New thermally stable energetic materials: synthesis and characterization of guanylhydrazone substituted furoxan energetic derivatives New Journal of Chemistry. ,vol. 39, pp. 179- 186 ,(2015) , 10.1039/C4NJ01175A
Thomas M. Klapötke, Tomasz G. Witkowski, Nitrogen‐Rich Energetic 1,2,5‐Oxadiazole‐Tetrazole – Based Energetic Materials Propellants, Explosives, Pyrotechnics. ,vol. 40, pp. 366- 373 ,(2015) , 10.1002/PREP.201400294
Chunlin He, Jean'ne M. Shreeve, Potassium 4,5‐Bis(dinitromethyl)furoxanate: A Green Primary Explosive with a Positive Oxygen Balance Angewandte Chemie. ,vol. 55, pp. 772- 775 ,(2016) , 10.1002/ANIE.201509209
L L Fershtat, N N Makhova, Advances in the synthesis of non-annelated polynuclear heterocyclic systems comprising the 1,2,5-oxadiazole ring Russian Chemical Reviews. ,vol. 85, pp. 1097- 1145 ,(2016) , 10.1070/RCR4619
Chunlin He, Yongxing Tang, Lauren A. Mitchell, Damon A. Parrish, Jean'ne M. Shreeve, N-Oxides light up energetic performances: synthesis and characterization of dinitraminobisfuroxans and their salts Journal of Materials Chemistry. ,vol. 4, pp. 8969- 8973 ,(2016) , 10.1039/C6TA03619H
N. N. Makhova, I. V. Ovchinnikov, V. S. Kuz'min, V. I. Pepekin, L. I. Khmel'nitskii, L. N. Akimova, DINITRODIAZENOFUROXAN AS A NEW ENERGETIC EXPLOSIVE Doklady Chemistry. ,vol. 359, pp. 67- 70 ,(1998)
Ilya V. Kuchurov, Mikhail N. Zharkov, Leonid L. Fershtat, Nina N. Makhova, Sergey G. Zlotin, Prospective Symbiosis of Green Chemistry and Energetic Materials Chemsuschem. ,vol. 10, pp. 3914- 3946 ,(2017) , 10.1002/CSSC.201701053