Application of quantitative 13C nuclear magnetic resonance spectroscopy to coal-derived materials

作者: William R. Ladner , Colin E. Snape

DOI: 10.1016/0016-2361(78)90016-9

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摘要: Abstract The difficulties associated with obtaining quantitative results from 13C nuclear magnetic resonance spectroscopy are discussed. By careful choice of the experimental conditions have been obtained for a mixture model compounds, containing most types carbon linkages present in coal-derived materials, and an aromatic fraction coal extract.

参考文章(7)
Otto A. Gansow, Aaron R. Burke, G. N. La Mar, A shiftless relaxation reagent for carbon-13 magnetic resonance of organometallic carbonyl compounds Journal of The Chemical Society, Chemical Communications. pp. 456- 457 ,(1972) , 10.1039/C39720000456
David L. Wooton, William M. Coleman, Larry T. Taylor, Harry C. Dorn, Characterization of organic fractions in solvent-refined coal by quantitative n.m.r. spectroscopy Fuel. ,vol. 57, pp. 17- 21 ,(1978) , 10.1016/0016-2361(78)90084-4
Ronald J. Pugmire, David M. Grant, Kurt W. Zilm, Larry L. Anderson, Alex G. Oblad, Ralph E. Wood, Carbon-13 magnetic resonance of coal-derived liquids Fuel. ,vol. 56, pp. 295- 301 ,(1977) , 10.1016/0016-2361(77)90011-4
James N. Shoolery, William L. Budde, Natural abundance carbon-13 nuclear magnetic resonance spectrometry for crude oil and petroleum product analyses Analytical Chemistry. ,vol. 48, pp. 1458- 1461 ,(1976) , 10.1021/AC50005A011
H. L. Retcofsky, F. K. Schweighardt, M. Hough, Determination of aromaticities of coal derivatives by nuclear magnetic resonance spectrometry and the Brown-Ladner equation Analytical Chemistry. ,vol. 49, pp. 585- 588 ,(1977) , 10.1021/AC50012A020
Keith D. Bartle, Terence G. Martin, Derek F. Williams, Chemical nature of a supercritical-gas extract of coal at 350 °C Fuel. ,vol. 54, pp. 226- 235 ,(1975) , 10.1016/0016-2361(75)90034-4
Harry C. Dorn, David L. Wooton, Analysis of hydrocarbon fractions by carbon and proton Fourier transform nuclear magnetic resonance spectrometry Analytical Chemistry. ,vol. 48, pp. 2146- 2148 ,(1976) , 10.1021/AC50008A023