Preparation and characterization of uniform nanocrystalline prismatic SnO2 particles
作者： M. Ocaña , C.J. Serna , E. Matijević
DOI: 10.1016/0167-577X(91)90052-8
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摘要: Abstract The preparation of nanosize prismatic SnO 2 particles fairly narrow size distribution by forced hydrolysis at 100°C acidic SnCl 4 solutions is described. are monocrystalline, with cassiterite structure having the c axis parallel to their longest dimension. thickness nanocrystals was evaluated infrared spectroscopy. Thermogravimetric study has shown that sintering starts temperatures several hundred degrees lower than conventional microcrystalline powders.
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