Fast and continuous synthesis of nanostructured iron spinel in supercritical water: influence of cations and citrates
作者： L. Maurizi , F. Bouyer , M. Ariane , R. Chassagnon , N. Millot
DOI: 10.1039/C4RA08562K
关键词:
摘要: Spinel iron oxide nanoparticles were obtained under supercritical water conditions in a continuous and fast (less than 10 s) way by modifying the initial stoichiometric FeII/FeIII molar ratio from (1/2) to (3/0), without base solution, using citrates directly with precursors. This result opens an economical environmentally benign approach synthesize superparamagnetic (SPIONs) high yields.
rsc.org
archives-ouvertes.fr
sci-hub.se 参考文章(54)
M. Iwasaki, M. Hara, S. Ito, Synthesis of nanometer-sized hematite single crystals through NAC-FAS method Journal of Materials Science. ,vol. 35, pp. 943- 949 ,(2000) , 10.1023/A:1004710810785
T. Belin, N. Millot, N. Bovet, M. Gailhanou, In situ and time resolved study of the γ/α-Fe2O3 transition in nanometric particles Journal of Solid State Chemistry. ,vol. 180, pp. 2377- 2385 ,(2007) , 10.1016/J.JSSC.2007.06.013
Dale?L. Huber, Synthesis, Properties, and Applications of Iron Nanoparticles Small. ,vol. 1, pp. 482- 501 ,(2005) , 10.1002/SMLL.200500006
Ji-Ho Park, Ki-Hyeong Im, Se-Ho Lee, Dong-Hyun Kim, Doug-Youn Lee, Yong-Keun Lee, Kwang-Mahn Kim, Kyoung-Nam Kim, Preparation and characterization of magnetic chitosan particles for hyperthermia application Journal of Magnetism and Magnetic Materials. ,vol. 293, pp. 328- 333 ,(2005) , 10.1016/J.JMMM.2005.02.027
T. Belin, N. Millot, F. Villiéras, O. Bertrand, J. P. Bellat, Structural variations as a function of surface adsorption in nanostructured particles Journal of Physical Chemistry B. ,vol. 108, pp. 5333- 5340 ,(2004) , 10.1021/JP0310899
Kiwamu Sue, Hayato Hattori, Toshiyuki Sato, Tomoe Komoriya, Akiko Kawai-Nakamura, Satoshi Tanaka, Toshihiko Hiaki, Shin-ichiro Kawasaki, Yoshihiro Takebayashi, Satoshi Yoda, Takeshi Furuya, Super-rapid Hydrothermal Synthesis of Highly Crystalline and Water-soluble Magnetite Nanoparticles Using a Microreactor Chemistry Letters. ,vol. 38, pp. 792- 793 ,(2009) , 10.1246/CL.2009.792
Catherine Pighini, Daniel Aymes, Nadine Millot, Lucien Saviot*, Low-frequency Raman characterization of size-controlled anatase TiO2 nanopowders prepared by continuous hydrothermal syntheses Journal of Nanoparticle Research. ,vol. 9, pp. 309- 315 ,(2007) , 10.1007/S11051-005-9061-6
Greta R. Patzke, Ying Zhou, Roman Kontic, Franziska Conrad, Oxide nanomaterials: synthetic developments, mechanistic studies, and technological innovations. Angewandte Chemie. ,vol. 50, pp. 826- 859 ,(2011) , 10.1002/ANIE.201000235
Lionel Maurizi, Usawadee Sakulkhu, Lindsey A. Crowe, Vanessa Mai Dao, Nicolas Leclaire, Jean-Paul Vallée, Heinrich Hofmann, Syntheses of cross-linked polymeric superparamagnetic beads with tunable properties RSC Advances. ,vol. 4, pp. 11142- 11146 ,(2014) , 10.1039/C3RA48004F
Seung-Ah Hong, Su Jin Kim, Kyung Yoon Chung, Youn-Woo Lee, Jaehoon Kim, Byung-In Sang, Continuous synthesis of lithium iron phosphate nanoparticles in supercritical water: Effect of process parameters Chemical Engineering Journal. ,vol. 229, pp. 313- 323 ,(2013) , 10.1016/J.CEJ.2013.05.094