Further study of tris(cyclohexyl)stannane compounds, Cy3SnX. Syntheses of the compounds with X=Br, I, N3 and NCS and redetermination of the crystal structures of Cy3SnX (X=Br and I)
作者： R. Alan Howie , Marcelo V.H. Moura , James L. Wardell , Solange M.S.V. Wardell
DOI: 10.1016/J.POLY.2004.08.001
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摘要: Abstract Methods of preparation and far IR data are presented for various Cy3SnX compounds. The synthesis tris(cyclohexyl)tin hydroxide, Cy3SnOH, is also described. Redeterminations the crystal structures bromide iodide, Cy3SnBr Cy3SnI, confirm their molecular nature improve considerably upon results reported earlier [S. Calogero, P. Ganis, V. Peruzzo, G. Tagliavini, Valle, J. Organomet. Chem. 220 (1981) 11] providing, in both cases, lower Rfactors and, particular, a revised estimate Sn–I bond length, now 2.7463(6) A.
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David Tudela, Ramón Fernández, Vitaly K. Belsky, Valery E. Zavodnik, Structural chemistry of triorganotin fluorides. The crystal structure of tricyclohexyltin fluoride revisited J. Chem. Soc., Dalton Trans.. pp. 2123- 2126 ,(1996) , 10.1039/DT9960002123
John Nicolson Low, James Wardell, João A. S. Bomfim, Solange M. S. V. Wardell, Chlorotris(2-methyl-2-phenylpropyl)tin(IV) at 150 K Acta Crystallographica Section C-crystal Structure Communications. ,vol. 56, ,(2000) , 10.1107/S0108270100015067
J. S. Tse, F. L. Lee, E. J. Gabe, Room-temperature and low-temperature structure of triphenyltin chloride Acta Crystallographica Section C-crystal Structure Communications. ,vol. 42, pp. 1876- 1878 ,(1986) , 10.1107/S0108270186090200
João A.S Bomfim, Carlos A.L Filgueiras, R Alan Howie, John N Low, Janet M.S Skakle, James L Wardell, Solange M.S.V Wardell, Tris(2-methyl-2-phenylpropyl)stannane derivatives, (Neo)3SnX, revisited. Comparison of crystal structures of (Neo)3SnX (X=Cl, Br, I, N3, NCS and OAc) Polyhedron. ,vol. 21, pp. 1667- 1676 ,(2002) , 10.1016/S0277-5387(02)01030-6
Frank H. Allen, The Cambridge Structural Database: a quarter of a million crystal structures and rising Acta Crystallographica Section B-structural Science. ,vol. 58, pp. 380- 388 ,(2002) , 10.1107/S0108768102003890
Robin K. Harris, Angelika. Sebald, Donatella. Furlani, Giuseppe. Tagliavini, High-resolution solid-state tin-119 NMR investigations of organotin halides R3SnX and R2SnX2 (R = alkyl, aryl; X = Cl, Br) Organometallics. ,vol. 7, pp. 388- 394 ,(1988) , 10.1021/OM00092A022
Sandro Calogero, Paolo Ganis, Valerio Peruzzo, Giuseppe Tagliavini, Crystal structure of tricyclohexyltin chloride Journal of Organometallic Chemistry. ,vol. 179, pp. 145- 152 ,(1979) , 10.1016/S0022-328X(00)95216-1
Sandro Calogero, Paolo Ganis, Valerio Peruzzo, Giuseppe Tagliavini, Giovanni Valle, X-ray and mössbauer studies of tricyclohexyltin(IV) halides. The crystal structures of (cyclo-C6H11)3SnX (X = F, Br and I) Journal of Organometallic Chemistry. ,vol. 220, pp. 11- 20 ,(1981) , 10.1016/S0022-328X(00)83099-5
L. J. Farrugia, ORTEP-3 for Windows - a version of ORTEP-III with a Graphical User Interface (GUI) Journal of Applied Crystallography. ,vol. 30, pp. 565- 565 ,(1997) , 10.1107/S0021889897003117
M. G. Simard, I. Wharf, Comparison of the structures of two trimesityltin iodide solvates and triphenyltin iodide Acta Crystallographica Section C-crystal Structure Communications. ,vol. 50, pp. 397- 403 ,(1994) , 10.1107/S0108270193008935