COMPARISON OF HEADSPACE SOLID PHASE MICROEXTRACTION AND XAD‐2 METHODS TO EXTRACT VOLATILE COMPOUNDS PRODUCED BY SACCHAROMYCES DURING WINE FERMENTATIONS
作者： JEFFRI C. BOHLSCHEID , XIAO-DONG WANG , D. SCOTT MATTINSON , CHARLES G. EDWARDS
DOI: 10.1111/J.1745-4557.2006.00052.X
关键词:
摘要: A modified headspace solid phase microextraction (HS-SPME) method was compared with Amberlite® XAD-2 resin for the extraction of volatile compounds. In HS-SPME method, volatiles were extracted using an 85 [mu]m polyacrylate fiber from wines that contained a standardized amount ethanol (10% v[solidus]v), NaCl (0.325 g[solidus]mL) and internal standards (dodecanol nonanoic acid). Both procedures yielded high relative recoveries (>92%) reproducibilities (coefficient variations
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