Improved determination of FID signal parameters in low-field NMR

作者: Juhani Dabek , Jaakko O. Nieminen , Panu T. Vesanen , Raimo Sepponen , Risto J. Ilmoniemi

DOI: 10.1016/J.JMR.2010.04.013

关键词:

摘要: In this work, novel methods are suggested for assessing signal parameters of the free induction decay (FID) in nuclear magnetic resonance (NMR) experiments. The FID was recorded a microtesla field and analysed to determine its relaxation time, amplitude, Larmor frequency phase. challenge posed by narrow line width, whose related effects were investigated through simulations, also. developed give new view on estimation as well lower higher fields. It is shown that transverse time sample can be accurately determined domain other means than Lorentz peak half width. Also, with some realistic approximations, simple functional form power spectrum shape proposed. As inspection instead absorption dispersion Lorentzians advantageous sense waveform independent automatic efficient presented work incorporate an integral exponential fit, fit two ways When there sufficiently many data points peak, provides quick, accurate way determining FID. measurements however, width led establishing more applicable method which based temporally moving window.

参考文章(30)
P Mutzenhardt, J Brondeau, F Humbert, D Canet, Algorithm based on a new proof of HSVD equations derived without invoking singular-value decomposition Journal of Magnetic Resonance. ,vol. 94, pp. 543- 549 ,(1991) , 10.1016/0022-2364(91)90140-O
H. Chen, S. Vanhuffel, C. Decanniere, P. Vanhecke, A Signal-Enhancement Algorithm for the Quantification of NMR Data in the Time Domain Journal of Magnetic Resonance, Series A. ,vol. 109, pp. 46- 55 ,(1994) , 10.1006/JMRA.1994.1133
Longqing Qiu, Yi Zhang, Hans-Joachim Krause, Alex I. Braginski, Martin Burghoff, Lutz Trahms, Nuclear magnetic resonance in the earth’s magnetic field using a nitrogen-cooled superconducting quantum interference device Applied Physics Letters. ,vol. 91, pp. 072505- ,(2007) , 10.1063/1.2771060
Hua Chen, Sabine Van Huffel, Dirk van Ormondt, Ron de Beer, Parameter Estimation with Prior Knowledge of Known Signal Poles for the Quantification of NMR Spectroscopy Data in the Time Domain Journal of Magnetic Resonance, Series A. ,vol. 119, pp. 225- 234 ,(1996) , 10.1006/JMRA.1996.0077
Yi Zhang, Longqing Qiu, Hans-Joachim Krause, Stefan Hartwig, Martin Burghoff, Lutz Trahms, Liquid state nuclear magnetic resonance at low fields using a nitrogen cooled superconducting quantum interference device Applied Physics Letters. ,vol. 90, pp. 182503- ,(2007) , 10.1063/1.2734896