Synthesis of Zn‐doped talc in hydrothermal atmosphere
作者： M. Catalano , E. Belluso , D. Miriello , E. Barrese , A. Bloise
关键词:
摘要: Zn-doped talc were synthesized under hydrothermal conditions at constant reaction time and pressure of 160 hours 2 kbar respectively, three different temperatures (300, 500 650 °C) with pH-values 5 7. The starting materials run products characterized by X-ray powder diffraction (XRPD), scanning electron microscopy annexed energy-dispersive spectrometry (SEM-EDS), differential calorimetry thermogravimetric analysis (DSC-TG) Fourier transform infrared (FT-IR). results showed that the temperature, pH-value mixture amount zinc in affected growth talc. When low temperature presents crystallinity, flawed morphology but higher content its lattice. A thermal treatment at, or above 500 °C allowed a significant flaw reduction morphology, crystallinity lower dopant. large amounts Zn present mixtures, grew small size poorly shaped. effect doping on some chemical/physical characteristics was also discussed.
sci-hub.se 参考文章(28)
Kiyotaka ISHIDA, Identification of infrared OH librational bands of talc-willemseite solid solutions and Al(IV)-free amphiboles through deuteration Mineralogical Journal. ,vol. 15, pp. 93- 104 ,(1990) , 10.2465/MINERJ.15.93
J. D. Russell, V. C. Farmer, B. Velde, Replacement of OH by OD in layer silicates, and identification of the vibrations of these groups in infra-red spectra Mineralogical Magazine. ,vol. 37, pp. 869- 879 ,(1970) , 10.1180/MINMAG.1970.037.292.01
Nabanita Pal, Manidipa Paul, Asim Bhaumik, Highly ordered Zn-doped mesoporous silica: An efficient catalyst for transesterification reaction Journal of Solid State Chemistry. ,vol. 184, pp. 1805- 1812 ,(2011) , 10.1016/J.JSSC.2011.05.033
Takayuki Hirai, Masanori Nanba, Isao Komasawa, Dithiol-mediated incorporation of CdS nanoparticles from reverse micellar system into Zn-doped SBA-15 mesoporous silica and their photocatalytic properties. joint international conference on information sciences. ,vol. 268, pp. 394- 399 ,(2003) , 10.1016/J.JCIS.2003.09.011
V Balek, J Šubrt, LA Pérez-Maqueda, M Beneš, IM Bountseva, IN Beckman, JL Pérez-Rodríguez, Thermal behavior of ground talc mineral Journal of Mining and Metallurgy, Section B. ,vol. 44, pp. 7- 17 ,(2008) , 10.2298/JMMB0801007B
F DELLISANTI, G VALDRE, M MONDONICO, Changes of the main physical and technological properties of talc due to mechanical strain Applied Clay Science. ,vol. 42, pp. 398- 404 ,(2009) , 10.1016/J.CLAY.2008.04.002
F. Martin, S. Petit, O. Grauby, M. P. Lavie, Gradual H/D substitution in synthetic germanium bearing talcs" a method for infrared band assignment Clay Minerals. ,vol. 34, pp. 365- 374 ,(1999) , 10.1180/000985599546154
Esteban F. Aglietti, The effect of dry grinding on the structure of talc Applied Clay Science. ,vol. 9, pp. 139- 147 ,(1994) , 10.1016/0169-1317(94)90033-7
M.M.A Ahmed, M.M., Ibrahim, G.A. and Hassan, None, Improvement of Egyptian talc quality for industrial uses by flotation process and leaching International Journal of Mineral Processing. ,vol. 83, pp. 132- 145 ,(2007) , 10.1016/J.MINPRO.2007.07.002
A Yu Pidluzhna, II Grigorchak, MV Nikipanchuk, BK Ostafiychuk, IM Budzulyak, MM Mitsov, LS Yablon’, None, Intercalation current generation in oxygen- and sulfur-doped talc Russian Journal of Electrochemistry. ,vol. 48, pp. 545- 549 ,(2012) , 10.1134/S1023193512040118